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| PHYSICO-MECHANICAL PROPERTIES VARIATION OF ROCK WITH PHASE TRANSFORMATION UNDER HIGH TEMPERATURE |
| SUN Qiang1,2,3,ZHANG Zhizhen2,XUE Lei3,ZHU Shuyun1 |
| (1. School of Resources and Earth Science,China University of Mining and Technology,Xuzhou,Jiangsu 221116,China;2. State Key Laboratory for Geomechanics and Deep Underground Engineering,China University of Mining and Technology,Xuzhou,Jiangsu 221116,China;3. Key Laboratory of Engineering Geomechanics,Institute of Geology and Geophysics,Chinese Academy of Sciences,Beijing 100029,China) |
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Abstract The change of rock internal microstructure along with temperature increasing leads to the variation of physico-mechanical properties. The experiments on physico-mechanical properties evolution of granite were carried out at temperature ranging from room temperature to 800 ℃ by using MTS servo-controlled testing machine and heating furnace. The research results indicate that:(1) The rock physico-mechanical properties change with temperature can be divided into five stages:i.e. room temperature to 100 ℃,100 ℃ to 300 ℃,300 ℃ to 500 ℃,500 ℃ to 600 ℃ and 600 ℃ to 800 ℃. The first three stages of temperature range correspond to the vaporization escaping interval of adhered water,and bound water and structural water. (2) The phsyico-mechanical parameters of rock have larger changes in temperature between 400 ℃ to 600 ℃,specially at the temperature of 573 ℃,where quartz has a phase transformation,from α phase to β phase. In this process,it is leaded to the increase of rock internal microcracks,which can be described as increasing of volume,reducing of bearing capacity,increasing of permeability,and the mutation of wave velocity. (3) After the temperature higher than 600 ℃,rock strength and wave velocity continue to reduce,which is influenced by solid mineral inflation and fracture of metallic bonding.
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Received: 13 November 2012
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| [1] WONG T F,BRACE W F. Thermal expansion of rocks:some measurements at high pressure[J]. Tectonophysics,1979,57(2/4):95–117.
[2] CHEN Y,WANG C Y. Thermally induced acoustic emission in Westerly granite[J]. Geophysical Research Letters,1980,7(12):1 089– 1 092.
[3] 陈 颙,吴晓东,张福勤. 岩石热开裂的实验研究[J]. 科学通报,1999,44(8):880–883.(CHEN Yong,WU Xiaodong,ZHANG Fuqin. Experimental research on rock thermal cracking[J]. Chinese Science bulletin,1999,44(8):880–883.(in Chinese))
[4] 赵阳升,郤保平,万志军,等. 高温高压下花岗岩中钻孔变形失稳临界条件[J]. 岩石力学与工程学报,2009,28(5):865–874.(ZHAO Yangsheng,XI Baoping,WAN Zhijun,et al. Study of critical condition of borehole instability in granite under high temperature and high pressure[J]. Chinese Journal of Rock Mechanics and Engineering,2009,28(5):865–874.(in Chinese))
[5] 张 渊,赵阳升,万志军,等. 不同温度条件下孔隙压力对长石细砂岩渗透率影响试验研究[J]. 岩石力学与工程学报,2008,27(1):53–58.(ZHANG Yuan,ZHAO Yangsheng,WAN Zhijun,et al. Experimental study of effect of pore pressure on feldspar fine sandstone permeability under different temperatures[J]. Chinese Journal of Rock Mechanics and Engineering,2008,27(1):53–58.(in Chinese))
[6] 武晋文. 花岗岩热破裂实验研究[硕士学位论文][D]. 太原:太原理工大学,2008.(WU Jinwen. An experimental research on granite heat cracking[M. S. Thesis][D]. Taiyuan:Taiyuan University of Technology,2008.(in Chinese))
[7] 王广地. 北山花岗岩温度效应试验研究及黏弹塑性分析[硕士学位论文][D]. 西安:西安科技学院,2003.(WANG Guangdi. Experiment research on the effects of temperature and viscoelastoplastic analysis of Beishan granite[M. S. Thesis][D]. Xi?an:Xi?an Institute of Science and Technology,2003.(in Chinese))
[8] 张静华,王静涛,赵爱国. 高温下花岗岩断裂特性的研究[J]. 岩土力学,1987,8(4):11–16.(ZHANG Jinghua,WANG Jingtao,ZHAO Aiguo. Fracture properties of granite at high temperature[J]. Rock and Soil Mechanics,1987,8(4):11–16.(in Chinese))
[9] 许锡昌. 花岗岩热损伤特性研究[J]. 岩土力学,2003,24(增2):188–191.(XU Xichang. Study on the characteristics of thermal damage for granite[J]. Rock and Soil Mechanics,2003,24(Supp.2):188–191.(in Chinese))
[10] 陈有亮,邵 伟,周有成. 高温作用后花岗岩力学性能试验研究[J]. 力学季刊,2011,32(3):397–402.(CHEN Youliang,SHAO Wei,ZHOU Youcheng. Experimental study on mechanical properties of granite after high temperature[J]. Chinese Quarterly of Mechanics,2011,32(3):397–402.(in Chinese))
[11] 徐小丽. 温度载荷作用下花岗岩力学性质演化及其微观机制研究[博士学位论文][D]. 徐州:中国矿业大学,2008.(XU Xiaoli. Research on the mechanical characteristics and micromechanism of granite[Ph. D. Thesis][D]. Xuzhou:China University of Mining and Technology,2008.(in Chinese))
[12] 徐小丽,高 峰,沈晓明,等. 高温后花岗岩力学性质及微孔隙结构特征研究[J]. 岩土力学,2010,31(6):1 752–1 758.(XU Xiaoli,GAO Feng,SHEN Xiaoming,et al. Research on mechanical characteristics and micropore structure of granite under high- temperature[J]. Rock and Soil Mechanics,2010,31(6):1 752– 1 758.(in Chinese))
[13] 刘均荣,秦积舜,吴晓东. 温度对岩石渗透率影响的实验研究[J]. 中国石油大学学报:自然科学版,2001,25(4):51–53.(LIU Junrong,QIN Jishun,WU Xiaodong. Experimental study on relation between temperature and rock permeability[J]. Journal of China University of Petroeum:Natural Science,2001,25(4):51–53.(in Chinese))
[14] 梁 冰,高红梅,兰永伟. 岩石渗透率与温度关系的理论分析和试验研究[J]. 岩石力学与工程学报,2005,24(12):53–58.(LIANG Bing,GAO Hongmei,LAN Yongwei. Theoretical analysis and experimental study on relation between rock permeability and temperature[J]. Chinese Journal of Rock Mechanics and Engineering,2005,24(12):53–58.(in Chinese))
[15] 张志镇,高 峰,刘治军. 温度影响下花岗岩冲击倾向及其微细观机制研究[J]. 岩石力学与工程学报,2010,29(8):1 591–1 602. (ZHANG Zhizhen,GAO Feng,LIU Zhijun. Research on rockburst process and its microcosmic mechanism of granite considering temperature effect[J]. Chinese Journal of Rock Mechanics and Engineering,2010,29(8):1 591–1 602.(in Chinese))
[16] 张志镇,高 峰,徐小丽. 花岗岩单轴压缩的声发射特征及热力耦合模型[J]. 地下空间与工程学报,2010,6(1):70–74.(ZHANG Zhizhen,GAO Feng,XU Xiaoli. Acoustic emission characteristics and themodynamic coupling model of granite under uniaxial compression[J]. Chinese Journal of Underground Space and Engineering,2010,6(1):70–74.(in Chinese))
[17] 白利平,杜建国,刘 巍,等. 高温高压下斜长岩纵波速度与电阻率实验研究[J]. 地震学报,2002,24(6):638–646.(BAI Liping,DU Jianguo,LIU Wei,et al. The experimental studies on electrical conductivities and P-wave velocities of anorthosite at high pressure and high temperature[J]. Acta Seismologica Sinica,2002,24(6):638–646.(in Chinese))
[18] 周永胜,蒋海昆,何昌荣. 不同温压条件下居庸关花岗岩脆塑性转化与失稳型式的实验研究[J]. 中国地震,2002,18(4):389–400.(ZHOU Yongsheng,JIANG Haikun,HE Changrong. Experiments of brittle-plastic transition,modes of instability of Juyongguan granite at different T-P conditions[J]. Earthquake Research in China,2002,18(4):389–400.(in Chinese))
[19] 蒋海昆,张 流,周永胜. 不同温度条件下花岗岩变形破坏及声发射时序特征[J]. 地震,2000,20(3):87–94.(JIANG Haikun,ZHANG Liu,ZHOU Yongsheng. Characteristics of AE temporal sequences in the process of deformation and failure of granite at high pressure and different temperatures[J]. Earthquake,2000,20(3):87–94.(in Chinese))
[20] DOBSON D P,MEREDITH P G,BOON S A. Simulation of subduction zone seismicity by dehydration of serpentine[J]. Science,2002,298(15):1 407–1 420.
[21] JUNG H,GREEN H W,DOBRZHINETSKAYA L F. Intermediate- depth earthquake faulting by dehydration embitterment with negative volume change[J]. Nature,2004,428(1):545–549.
[22] 席道瑛. 花岗岩中矿物相变的物性特征[J]. 矿物学报,1994,14(3):223–227.(XI Daoying. Physical characteristics of mineral phase transition in the granite [J]. Acta Mineralogica Sinica,1994,14(3):223–227.(in Chinese))
[23] 傅国飞,徐洪武. 两种不同燧石中α–石英 β石英相变的研究[J]. 地质科学,1992,(1):50–54.(FU Guofei,XU Hongwu. A study of α-quartz β-quartz phase transition of two kinds of cherts[J]. Scientia Geologica Sinica,1992,(1):50–54.(in Chinese))
[24] 席道瑛,程经毅,黄建华. 声发射在研究岩石古温度中的应用[J]. 中国科学技术大学学报,1996,26(1):97–101.(XI Daoying,CHENG Jingyi,HUANG Jianhua. The application of acoustic emission in the study of ancient temperature of rock[J]. Journal of University of Science and Technology of China,1996,26(1):97–101.(in Chinese))
[25] 孙君秀,谢亦汉,张友南. 华北太古宙长英质岩石的地震波速度及其在地壳中的位置[J]. 地震学报,2000,22(6):622–631.(SUN Junxiu,XIE Yihan,ZHANG Younan. Seismic wave velocity of archeozoic felsic rocks from North China and its existing location in the crust[J]. Acta Seismologica Sinica,2000,22(6):622–631.(in Chinese))
[26] 赵忠魁,孙清州,张普庆,等. 高温焙烧对石英砂加热时的相变与膨胀性的影响[J]. 铸造,2006,55(9):961–964.(ZHAO Zhongkui,SUN Qingzhou,ZHANG Puqing,et al. Effect of calcinatin on phase transformation and expansibility of quartz sands during heating[J]. Foundry,2006,55(9):961–964.(in Chinese))
[27] 孙清州,赵忠魁,张普庆,等. 热再生石英砂改性机制[J]. 铸造,2005,54(10):1 025–1 026.(SUN Qingzhou,ZHAO Zhongkui,ZHANG Puqing,et al. Modification mechanism of properties of hot-reclaimed quartz sands[J]. Foundry,2005,54(10):1 025–1 026. (in Chinese))
[28] 张广强. 不同初始状态的SiO2在高温高压下的结构转变研究[博士学位论文][D]. 长春:吉林大学,2009.(ZHANG Guangqiang. Structural transformation of SiO2 with different initial states under high temperature and high pressure[Ph. D. Thesis][D]. Changchun:Jilin University,2009.(in Chinese)) |
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