(1. College of Mining Engineering,Taiyuan University of Technology,Taiyuan,Shanxi 030024,China;2. Key Laboratory of In-situ Property-improving Mining of Ministry of Education,Taiyuan University of Technology,Taiyuan,Shanxi 030024,China)
Abstract:To investigate the deformation and structure variation of lignite under the thermal-mechanical action,experiments were performed to the lignite samples of 50 mm in diameter and 100 mm in length with the high temperature and trixial stress testing platform. The structure variation was studied with Micro-CT,mercury intrusion and liquid nitrogen adsorption methods. Several fundamental characteristics of lignite deformation were obtained when the temperature rose from 23 ℃ to 400 ℃ at a rate of 3 ℃/min under the triaxial constant stress of 7 MPa. The deformation process of lignite can be divided into three stages:a slowly swelling stage with the temperature rising from 23 ℃ to 170 ℃,a rapidly compressing stage with the temperature rising from 170 ℃ to 289 ℃ and a relatively slowly compressing stage with the temperature rising from 289 ℃ to 400 ℃. The critical temperature of the brittle-ductile transition for lignite is about 180 ℃. During the constant load and temperature process,the final value of the axial strain increased firstly then decreased with the largest value of 2.5% at 200 ℃ and the smallest value of about 1.3% at 100 ℃. The largest total radial strain is about 19% and the largest total volume strain is about 41% at 400 ℃. The lignite deformation has great effect on its structure evolution. The total porosity of lignite increased firstly then decreased with the temperature rising. The largest total porosity is 21.46% at 200 ℃ while the smallest total porosity is only 7.61% at 23 ℃. The diameter of the main fissures increased with the temperature rising. The lignite porosity in the heating process has good fractal characteristics. The fractal dimension value decreased firstly then increased while the value of lnA0 increased firstly then decreased with the temperature rising.
[1] 赵阳升. 多孔介质多场耦合作用及其工程响应[M]. 北京:科学出版社,2010:374.(ZHAO Yangsheng. Multi-field coupling function and engineering response of porous media[M]. Beijing:Science Press,2010:374.(in Chinese))
[2] 周建勋,王桂梁,邵震杰. 煤的高温高压实验变形研究[J]. 煤炭学报,1994,19(3):324–331.(ZHOU Jianxun,WANG Guiliang,SHAO Zhenjie. Coal deformation under high temperature and confining pressure[J]. Journal of China Coal Society,1994,19(3):324–331.(in Chinese))
[3] 周建勋,王桂梁,邵震杰. 煤高温高压变形试验及其构造地质意义[J]. 地球物理学进展,1993,8(4):54–60.(ZHOU Jianxun,WANG Guiliang,SHAO Zhenjie. Coal deformation experiment underhigh temperature and confining pressure and its tectonic implications[J]. Progress in Geophysics,1993,8(4):54–60.(in Chinese))
[4] 周长冰,万志军,张 源,等. 气煤热力耦合变形与孔隙衍化特征的实验研究[J]. 中南大学学报:自然科学版,2014,45(7):2 440– 2 446.(ZHOU Changbing,WAN Zhijun,ZHANG Yuan,et al. Experimental study on coupled hermo-mechanical deformation and pore evolution feature of gas coal[J]. Journal of Central South University:Science and Technology,2014,45(7):2 440–2 446.(in Chinese))
[5] 冯子军,赵阳升,万志军,等. 热力耦合作用下无烟煤煤体变形特征的试验研究[J]. 岩石力学与工程学报,2010,29(8):1 624–1 630. (FENG Zijun,ZHAO Yangsheng,WAN Zhijun,et al. Experimental investigation into deformation characteristics of anthracite under thermo-mechanical coupling conditions[J]. Chinese Journal of Rock Mechanics and Engineering,2010,29(8):1 624–1 630.(in Chinese))
[6] 姜 波,秦 勇,金法礼. 煤变形的高温高压实验研究[J]. 煤炭学报,1997,22(1):80–84.(JIANG Bo,QIN Yong,JIN Fali. Coal deformation test under high temperature and confining pressure[J]. Journal of China Coal Society,1997,22(1):80–84.(in Chinese))
[7] 金法礼,秦 勇. 高温高压下煤变形的实验分析[J]. 煤田地质与勘探,1999,27(1):13–16.(JIN Fali,QIN Yong. Coal deformation test under high temperature and confining pressure[J]. Coal Geology and Exploration,1999,27(1):13–16.(in Chinese))
[8] 万志军,冯子军,赵阳升,等. 高温三轴应力下煤体弹性模量的演化规律[J]. 煤炭学报,2011,36(10):1 736–1 740.(WAN Zhijun,FENG Zijun,ZHAO Yangsheng,et al. Elastic modulus?s evolution law of coal under high temperature and triaxial stress[J]. Journal of China Coal Society,2011,36(10):1 736–1 740.(in Chinese))
[9] YU Y M,LIANG W G,HU Y Q,et al. Study of micro-pores development in lean coal with temperature[J]. International Journal of Rock Mechanics and Mining Sciences,2012,51:91–96.
[10] 孟巧荣,赵阳升,胡耀青,等. 褐煤热破裂的显微CT实验[J]. 煤炭学报,2011,36(5):855–860.(MENG Qiaorong,ZHAO Yangsheng,HU Yaoqing,et al. Micro-CT experimental of the thermal cracking of brown coal[J]. Journal of China Coal Society,2011,36(5):855–860. (in Chinese))
[11] TOMECZEK J,GIL S. Volatiles release and porosity evolution during high pressure coal pyrolysis[J]. Fuel,2003,82(3):285–292.
[12] 张志镇,高 峰,高亚楠,等. 高温影响下花岗岩孔径分布的分形结构及模型[J]. 岩石力学与工程学报,2016,35(12):2 426–2 438. (ZHANG Zhizhen,GAO Feng,GAO Yanan,et al. Fractal sreucture and model of pore size distribution of granite under high temperature[J]. Chinese Journal of Rock Mechanics and Engineering,2016,35(12):2 426–2 438.(in Chinese))
[13] 牛世伟. 褐煤热重分析与恒温失重特性研究[J]. 煤炭技术,2015,34(12):263–264.(NIU Shiwei. Investigation of pyrolysis and thermostatic weight loss properties of lignite[J]. Coal Technology,2015,34(12):263–264.(in Chinese))
[14] 徐忠和,赵阳升,杨 栋,等. 乌兰察布褐煤的热解产气与改性特征[J]. 辽宁工程技术大学学报:自然科学版,2016,35(5):460–463.(XU Zhonghe,ZHAO Yangsheng,YANG Dong,et al. Experimental investigation for pyrolysis gas and modification characteristics of Wulanchabu lignite under high temperature triaxial stress[J]. Journal of Liaoning Technical University:Natural Science,2016,35(5):460–463.(in Chinese))
[15] 谢克昌. 煤的结构与反应性[M]. 北京:科学出版社,2002:44.(XIE Kechang. Coal structure and its reactivity[M]. Beijing:Science Press,2002:44.(in Chinese))