(1. College of Mining Engineering,Taiyuan University of Technology,Taiyuan,Shanxi 030024,China;2. Key Laboratory of
In-situ Property-improving Mining of Ministry of Education,Taiyuan University of Technology,Taiyuan,Shanxi 030024,China)
Abstract:In order to study the effects of loading strain rate and supercritical CO2 on the mechanical properties of coal rock,uniaxial compression experiments of un-soaked and supercritical CO2 soaked coal rock are carried out under different quasi-static strain rate(10-5,10-4,10-3,10-2 s-1) loading. The energy signals during the loading process are recorded by acoustic emission monitoring system. The uniaxial compressive strength,elastic modulus,failure mode,energy evolution and AE characteristic parameters of the tested coal rock are studied from the perspective of strain rate effect and ScCO2 soaking weakened mechanism. The results show that:(1) With the increase of the loading strain rate,the compressive strength and elastic modulus of the un-soaked and supercritical CO2-soaked coal rock increase at first and decrease later. Under the loading strain rates of 10-5 and 10-2 s-1,the deterioration of mechanical properties of coal soaked in supercritical CO2 is more obvious. The uniaxial compressive strength of coal rock is reduced by 28.66% and 34.98%,and the corresponding elastic modulus is reduced by 35.50% and 27.68%,respectively. (2) The failure mode of un-soaked supercritical CO2 coal rock is mainly in the style of the X-shaped conjugated shear failure,while the failure mode of the supercritical CO2 soaked coal rock changes from inclined shear failure to vertical splitting tensile failure with the loading rate increase. (3) Both the loading strain rate and ScCO2 have effects on the mechanical properties of coal and rock. They also affect the elastic strain energy stored in the tested coal rock. It can be proved from the measured acoustic emission signal which characterizes the energy release during the failure process of the coal rock. This study is not only meaningful for revealing the variation law of mechanical properties of the supercritical CO2-soaked coal rock under different loading rates,but also helpful for understanding the coal rock deformation and fracture characteristics during fracturing of coal reservoirs.
[1] 王 磊,梁卫国. 超临界CO2/清水压裂煤体起裂和裂缝扩展试验研究[J]. 岩石力学与工程学报,2019,38(增1):2 680–2 689.(WANG Lei,LIANG Weiguo. Experimental study on fracture initiation and growth in coal using hydraulic fracturing with supercritical CO2 and normal water[J]. Chinese Journal of Rock Mechanics and Engineering,2019,38(Supp.1):2 680–2 689.(in Chinese))
[2] 梁卫国,张倍宁,黎 力,等. 注能(以CO2为例)改性驱替开采CH4理论与实验研究[J]. 煤炭学报,2018,43(10):2 839–2 847.(LIANG Weiguo,ZHANG Beining,LI Li,et al. Theory and experimental study of CBM recovery driven by energy boosting[J]. Journal of China Coal Society,2018,43(10):2 839–2 847.(in Chinese))
[3] 尹小涛,葛修润,李春光,等. 加载速率对岩石材料力学行为的影响[J]. 岩石力学与工程学报,2010,29(增1):2 610–2 615.(YIN Xiaotao,GE Xiurun,LI Chunguang,et al. Influences of loading rates on mechanical behaviors of rock materials[J]. Chinese Journal of Rock Mechanics and Engineering,2010,29(Supp.1):2 610–2 615.(in Chinese))
[4] LIANG C,WU S,LI X,et al. Effects of strain rate on fracture characteristics and mesoscopic failure mechanisms of granite[J]. International Journal of Rock Mechanics and Mining Sciences,2015,76:146–154.
[5] LIU X,LIU Z,LI X,et al. Experimental study on the effect of strain rate on rock acoustic emission characteristics[J]. International Journal of Rock Mechanics and Mining Sciences,2020,133(1):104420.
[6] 宫凤强,叶 豪,罗 勇. 低加载率范围内煤岩组合体冲击倾向性的率效应试验研究[J]. 煤炭学报,2017,42(11):2 852–2 860. (GONG Fengqiang,YE Hao,LUO Yong. Rate effect on the burst tendency of coal-rock combined body under low loading rate range[J]. Journal of China Coal Society,2017,42(11):2 852–2 860.(in Chinese))
[7] LU Z G,JU W,GAO F,et al. Influence of loading rate on the failure characteristics of composite coal-rock specimens under quasi-static loading conditions[J]. Rock Mechanics and Rock Engineering,2022,55(2):909–921.
[8] GAO M,XIE J,GAO Y,et al. Mechanical behavior of coal under different mining rates:A case study from laboratory experiments to field testing[J]. International Journal of Mining Science and Technology,2021,31(5):825–841.
[9] 李海涛,蒋春祥,姜耀东,等. 加载速率对煤样力学行为影响的试验研究[J]. 中国矿业大学学报,2015,44(3):430–436.(LI Haitao,JIANG Chunxiang,JIANG Yaodong,et al. Mechanical behavior and mechanism analysis of coal samples based on loading rate[J]. Journal of China University of Mining and Technology,2015,44(3):430–436.(in Chinese))
[10] 谢 晶,高明忠,张 盛,等. 深部煤岩三轴破断行为与能量释放的加载率效应试验研究[J]. 中南大学学报:自然科学版,2021,52(8):2 713–2 724.(XIE Jing,GAO Mingzhong,ZHANG Sheng,et al. Experimental study on triaxial fracture behavior and energy release law of deep coal under the effect of loading rates[J]. Journal of Central South University:Science and Technology,2021,52(8):2 713–2 724.(in Chinese))
[11] 刘晓辉,郑 钰,郝齐钧,等. 基于特征应力的准静态三轴煤岩脆性特征分析[J]. 岩石力学与工程学报,2021,40(12):2 454–2 565. (LIU Xiaohui,ZHENG Yu,HAO Qijun,et al. Quasi-static triaxial coal and rock brittleness analysis based on characteristic stress[J]. Chinese Journal of Rock Mechanics and Engineering,2021,40(12):2 454–2 565.(in Chinese))
[12] 刘晓辉,郝齐钧,吴世勇,等. 准静态应变率下的煤岩非线性力学特性[J]. 煤炭学报,2019,44(5):1 437–1 445.(LIU Xiaohui,HAO Qijun,WU Shiyong,et al. Nonlinear mechanical properties of coal rock under quasi-static strain rate[J]. Journal of China Coal Society,2019,44(5):1 437–1 445.(in Chinese))
[13] KUN Z,WUSHENG Z,CHANGKUN Q,et al. Experimental study on the mechanical behavior and failure characteristics of layered coal at medium strain rates[J]. Energies,2021,14(20):6 616.
[14] 唐一举,郝天轩,李 帆,等. 考虑应变速率效应的煤岩能量演化和红外辐射特征分析研究[J]. 岩石力学与工程学报,2022,41(6):1 126–1 135.(TANG Yiju,HAO Tianxuan,LI Fan,et al. Energy evolution and infrared radiation characterization of coal rocks considering strain rate effect[J]. Chinese Journal of Rock Mechanics and Engineering,2022,41(6):1 126–1 135.(in Chinese))
[15] PERERA M S A,RANJITH P G,VIETE D R. Effects of gaseous and super-critical carbon dioxide saturation on the mechanical properties of bituminous coal from the Southern Sydney Basin[J]. Applied Energy,2013,110:73–81.
[16] PERERA M S A,RANJITH P G,PETER M. Effects of saturation medium and pressure on strength parameters of Latrobe Valley brown coal:Carbon dioxide,water and nitrogen saturations[J]. Energy,2011,36(12):6 941–6 947.
[17] 张倍宁. 超临界CO2在不同阶煤层中的渗流规律及煤体变形特征研究[博士学位论文][D]. 太原:太原理工大学,2019.(ZHANG Beining. Investigation of supercritical CO2 flow behavior and mechanical deformation in different rank coals[Ph. D. Thesis][D]. Taiyuan:Taiyuan University of Technology,2019.(in Chinese))
[18] 何 江. 煤矿采动动载对煤岩体的作用及诱冲机制研究[博士学位论文][D]. 徐州:中国矿业大学,2013.(HE Jiang. Research of mining dynamic loading effect and its induced rock burst in coal mine[Ph. D. Thesis][D]. Xuzhou:China University of Mining and Technology,2013.(in Chinese))
[19] 乔纳斯A,朱卡斯. 碰撞动力学[M]. 张志云,丁世用译. 北京:兵器工业出版社,1989:327–329.(JONAS A,Zukas. Impact dynamics[M]. Translated by ZHANG Zhiyun,DING Shiyong. Beijing:Publishing House of Ordnance Industry,1989:327–329.(in Chinese))
[20] 赵阳升. 矿山岩石流体力学[M]. 北京:煤炭工业出版社,1994:112–114.(ZHAO Yangsheng. Rock fluid mechanics in Mine[M]. Beijing:China Coal Industry Publishing House,1994:112–114.(in Chinese))
[21] YU Y,ZHU W,LI L,et al. Multi-fracture interactions during two-phase flow of oil and water in deformable tight sandstone oil reservoirs[J]. Journal of Rock Mechanics and Geotechnical Engineering,2020,12(4):821–849.
[22] OLIVER B,TIM V D V,TIM B,et al. A reduced integration-based solid-shell finite element formulation for gradient-extended damage[J]. Computer Methods in Applied Mechanics and Engineering,2021,382(1):113884.
[23] 贺 伟,梁卫国,张倍宁,等. 不同煤阶煤体吸附储存CO2膨胀变形特性试验研究[J]. 煤炭学报,2018,43(5):1 408–1 415.(HE Wei,LIANG Weiguo,ZHANG Beining. et al. Experimental study on swelling characteristics of CO2 and storage in different coal rank[J]. Journal of China Coal Society,2018,43(5):1 408–1 415.(in Chinese))
[24] 桑树勋,牛庆合,曹丽文,等. 深部煤层CO2注入煤岩力学响应特征及机制研究进展[J]. 地球科学,2022,47(5):1 849–1 864.(SANG Shuxun,NIU Qinghe,CAO Liwen,et al. Mechanical response characteristics and mechanism of coal-rock with CO2 Injection in deep coal seam:A review[J]. Earth Science,2022,47(5):1 849–1 864.(in Chinese))
[25] KARACAN C Ö. Swelling-induced volumetric strains internal to a stressed coal associated with CO2 sorption[J]. International Journal of Coal Geology,2007,72(3/4):209–220.
[26] LARSEN J W. The effects of dissolved CO2 on coal structure and properties[J]. International Journal of Coal Geology,2003,57(1):63–70.
[27] 刘 斌,赵毅鑫,张 汉,等. 单轴压缩及劈裂试验下煤的声发射特征研究[J]. 采矿与安全工程学报,2020,37(3):613–621.(LIU Bin,ZHAO Yixin,ZHANG Han,et al. Acoustic emission characteristics of coal under uniaxial compression and Brazilian splitting[J]. Journal of Mining and Safety Engineering,2020,37(3):613–621.(in Chinese))
[28] NIU Q,WANG Q,WANG W,et al. Responses of multi-scale microstructures,physical-mechanical and hydraulic characteristics of roof rocks caused by the supercritical CO2-water-rock reaction [J]. Energy,2022,238(PartB):121727.
[29] NIU Q,CAO L,SANG S,et al. Experimental study on the softening effect and mechanism of anthracite with CO2 injection[J]. International Journal of Rock Mechanics and Mining Sciences,2021,138:104614.
[30] 梁卫国,贺 伟,阎纪伟. 超临界CO2致煤岩力学特性弱化与破裂机制[J]. 煤炭学报,2022,47(7):2 557–2 568.(LIANG Weiguo,HE Wei,YAN Jiwei. Weakening and fracturing mechanism of properties of coal and rock by supercritical CO2[J]. Journal of China Coal Society,2022,47(7):2 557–2 568.(in Chinese))
[31] 王 恬,桑树勋,刘世奇,等. ScCO2-H2O作用下不同煤级煤化学结构变化的实验研究[J]. 煤田地质与勘探,2018,46(5):60–65.(WANG Tian,SANG Shuxun,LIU Shiqi,et al. Experiment study on the chemical structure changes of different rank coals under action of supercritical carbon dioxide and water[J]. Coal Geology and Exploration,2018,46(5):60–65.(in Chinese))
[32] 姜仁霞,于洪观,王 力. 基于煤层封存CO2的煤中有机质超临界CO2萃取试验装置的建立[J]. 煤炭学报,2016,41(3):680–686.(JIANG Renxia,YU Hongguan,WANG Li. Development of an apparatus for the supercritical CO2 extraction of organic matter from coal based on CO2 sequestration in coal seams[J]. Journal of China Coal Society,2016,41(3):680–686.(in Chinese))
[33] ZHANG K,CHENG Y,LI W,et al. Influence of supercritical CO2 on pore structure and functional groups of coal:Implications for CO2 sequestration[J]. Journal of Natural Gas Science and Engineering,2017,40:288–298.
[34] RANATHUNGA A S,PERERA M,RANJITH P G,et al. Super-critical CO2 saturation-induced mechanical property alterations in low rank coal:An experimental study[J]. The Journal of Supercritical Fluids,2015,109:134–140.
[35] 谢和平,鞠 杨,黎立云. 基于能量耗散与释放原理的岩石强度与整体破坏准则[J]. 岩石力学与工程学报,2005,24(17):3 003–3 010. (XIE Heping,JU Yang,LI Liyun. Criteria for strength and structural failure of rocks based on energy dissipation and energy release principles[J]. Chinese Journal of Rock Mechanics and Engineering,2005,24(17):3 003–3 010.(in Chinese))
[36] QIN X,DAOLONG C,XILING L,et al. Research on the effect of loading rate on the fracture characteristics of granite using cracked straight through Brazilian disc specimens[J]. Theoretical and Applied Fracture Mechanics,2022,122:103581.