Static mechanical properties and microstructural damage characteristics of CO2 adsorbed coal mass
WANG Lei,ZHANG Yu,ZHU Chuanqi,LIU Huaiqian,CHEN Lipeng,LI Shaobo,WU Yuxuan
(State Key Laboratory of Mining Response and Disaster Prevention and Control in Deep Coal Mine,Anhui University of Science and Technology,Huainan,Anhui 232001,China)
Abstract:In order to explore the influence of different CO2-load coupling effects on the mechanical properties and meso-damage and failure characteristics of coal mass,the uniaxial loading tests of raw coal under different CO2 pressures were carried out by using industrial CT scanning system,MTS 816 rock mechanics loading device and self-developed gas-solid coupling test device. The influence of CO2 pressure on the mechanical properties and failure mode of coal was analyzed. Based on image processing technology,the meso-damage evolution characteristics and crack propagation laws of coal bodies are explored from two-dimensional and three-dimensional scales respectively,and the mechanical response mechanism of coal bodies to CO2-load coupling is revealed from the macro-meso-level. The results indicate that:(1) the stress-strain curve of coal mass under gas-solid coupling can be divided into four typical stages,and both peak strength and elastic modulus exhibited a degradation trend with increasing initial CO2 pressure. (2) Coal fracture expansion can be divided into fracture adsorption and expansion stage,fracture compaction and closing stage,new fracture initiation and development stage,and fracture rapid expansion and penetration stage,the fracture volume,fracture rate and three-dimensional fractal dimension are positively correlated with CO2 pressure,additionally,influenced by the CO2 gas wedge effect,the spatial distribution of fractures inside the loaded coal mass becomes complex,and its failure form gradually changes from a single tension failure to a compound failure in which tension and shear coexist. (3) The damage variable was defined based on three-dimensional porosity,and it was found that its value gradually increased from 0 to 0.34,approximately exhibiting an exponential rise. By comparing the peak strength of the coal under gas-solid coupling with the theoretical strength obtained from the damage variable,the rationality of the damage variable was validated.
[1] 肖 畅,王 开,张小强,等. 超临界CO2作用后无烟煤力学损伤演化特性及机制[J]. 煤炭学报,2022,47(6):2 340–2 351.(XIAO Chang,WANG Kai,ZHANG Xiaoqiang,et al. Mechanical damage evolution characteristics and mechanism of anthracite treated with supercritical CO2[J]. Journal of China Coal Society,2022,47(6):2 340–2 351.(in Chinese))
[2] 刘延锋,李小春,白 冰. 中国CO2煤层储存容量初步评价[J]. 岩石力学与工程学报,2005,24(16):2 947–2 952.(LIU Yanfeng,LI Xiaochun,BAI Bing. Preliminary estimation of CO2 storage capacity of coalbeds in China[J]. Chinese Journal of Rock Mechanics and Engineering,2005,24(16):2 947–2 952.(in Chinese))
[3] 何学秋,王恩元,林海燕. 孔隙气体对煤体变形及蚀损作用机理[J]. 中国矿业大学学报,1996,25(1):6–11.(HE Xueqiu,WANG Enyuan,LIN Haiyan. Coal deformation and fracture mechanism under pore gas action[J]. Journal of China University of Mining and Technology,1996,25(1):6–11.(in Chinese))
[4] 孙泽东,冯 淦,宋选民,等. CO2状态与各向异性对烟煤渐进破坏特征影响的实验研究[J]. 岩石力学与工程学报,2022,41(1):70–81.(SUN Zedong,FENG Gan,SONG Xuanmin,et al. Effects of CO2 state and anisotropy on the progressive failure characteristics of bituminous coal:an experimental study[J]. Chinese Journal of Rock Mechanics and Engineering,2022,41(1):70–81.(in Chinese))
[5] 张庆贺,杨 科,袁 亮,等. 吸附性气体对构造煤的损伤效应试验研究[J]. 采矿与安全工程学报,2019,36(5):995–1 001.(ZHANG Qinghe,YANG Ke,YUAN Liang,et al. Experimental study on damage effect of adsorbed gas on structural coal[J]. Journal of Mining and Safety Engineering,2019,36(5):995–1 001.(in Chinese))
[6] 朱川曲,马合意,赵鹏涛. 吸附CO2煤体的力学性能劣化机制[J]. 过程工程学报,2022,22(12):1 676–1 682.(ZHU Chuanqu, MA Heyi,ZHAO Pengtao. Degradation mechanism of mechanical properties for CO2 adsorbed coal[J]. The Chinese Journal of Process Engineering,2022,22(12):1 676–1 682.(in Chinese))
[7] 李清川,王汉鹏,袁 亮,等. 吸附气体量对煤岩力学特性损伤劣化的试验研究[J]. 中国矿业大学学报,2019,48(5):955–965.(LI Qingchuan,WANG Hanpeng,YUAN Liang,et al. Experimental study of damage and degradation of coal by adsorbed gas amount[J]. Journal of China University of Mining and Technology,2019,48(5):955–965.(in Chinese))
[8] VIETE D R,RANJITH P G. The effect of CO2 on the geomechanical and permeability behaviour of brown coal:Implications for coal seam CO2 sequestration[J]. International Journal of Coal Geology,2006,66(3):204–216.
[9] VIETE D R,RANJITH P G. The mechanical behaviour of coal with respect to CO2 sequestration in deep coal seams [J]. Fuel,2007,86(17):2 667–2 671.
[10] PERERA M S A,RANJITH P G,VIETE D R. Effects of gaseous and super-critical carbon dioxide saturation on the mechanical properties of bituminous coal from the Southern Sydney Basin[J]. Applied Energy,2013,110:73–81.
[11] 许 江,冯 丹,程立朝,等. 含瓦斯煤剪切破裂过程细观演化[J]. 煤炭学报,2014,39(11):2 213–2 219.(XU Jiang,FENG Dan,CHENG Lichao,et al. Mesoscopic evolution of coal containing gas?s shear fracture[J]. Journal of China Coal Society,2014,39(11):2 213–2 219.(in Chinese))
[12] 彭守建,许 江,张超林,等. 含瓦斯煤岩剪切破断过程中裂纹演化及其分形特征[J]. 煤炭学报,2015,40(4):801–808.(PENG Shoujian, XU Jiang, ZHANG Chaolin,et al. Fractal characteristics of crack evolution in gas-bearing coal under shear loading[J]. Journal of China Coal Society,2015,40(4):801–808.(in Chinese))
[13] 曹树刚,刘延保,李 勇,等. 煤岩固–气耦合细观力学试验装置的研制[J]. 岩石力学与工程学报,2009,28(8):1 681–1 690.(CAO Shugang, LIU Yanbao, LI Yong,et al. Research and development of testing apparatus of coal solid-gas coupled meso-mechanics[J]. Chinese Journal of Rock Mechanics and Engineering,2009,28(8):1 681–1 690.(in Chinese))
[14] 王 磊,商瑞豪,刘怀谦,等. 含多裂隙煤体裂纹细观演化规律与相互作用机制[J]. 中国矿业大学学报,2023,52(2):300–313.(WANG Lei, SHANG Ruihao, LIU Huaiqian,et al. Microcrack evolution law and interaction mechanism of coal with multiple cracks[J]. Journal of China University of Mining and Technology,2023,52(2):300–313.(in Chinese))
[15] 冯雪健,沈永星,周 动,等. 基于CT数字岩心深度学习的煤裂隙分布识别研究[J]. 煤炭科学技术,2023,51(8):97–104.(FENG Xuejian,SHEN Yongxing,ZHOU Dong,et al. Multi-scale distribution of coal fractures based on CT digital core deep learning[J]. Coal Science and Technology,2023,51(8):97–104.(in Chinese))
[16] 郝晨光,郭晓阳,邓存宝,等. 基于Bi-PTI模型的CT数字煤岩孔裂隙精准识别及阈值反演[J]. 煤炭学报,2023,48(4):1 516–1 526. (HAO Chenguang,GUO Xiaoyang,DENG Cunbao,et al. Precise identification and threshold inversion of pores and fissures in CT digital coal rock based on Bi-PTI model[J]. Journal of China Coal Society,2023,48(4):1 516–1 526.(in Chinese))
[17] 冯龙飞,王双明,王 海,等. 彬长矿区典型顶板水害矿井洛河组砂岩微观孔隙特征研究[J]. 煤炭科学技术,2023,51(8):208–218.(FENG Longfei,WANG Shuangming,WANG Hai,et al. Micro pore characteristics of Luohe aquifer sandstone in Binchang mining area typical roof water hazard mines[J]. Coal Science and Technology,2023,51(8):208–218.(in Chinese))
[18] 谭 皓,宋勇军,郭玺玺,等. 冻融裂隙砂岩细观损伤与应变局部化研究[J]. 岩石力学与工程学报,2022,41(12):2 485–2 496.(TAN Hao,SONG Yongjun,GUO Xixi,et al. Research on meso-damage and strain localization of fractured sandstone after freeze-thaw cycles[J]. Chinese Journal of Rock Mechanics and Engineering,2022,41(12):2 485–2 496.(in Chinese))
[19] 张 良,齐庆新,REN Ting,等. 基于显微CT扫描和统计强度的煤岩损伤破裂特性研究[J]. 煤炭科学技术,2023,51(增1):1–12.(ZHANG Liang,QI Qingxin,REN Ting,et al. Study on the damage and fracture characteristics of coal rock based on the X-ray micro-CT scanning technology and statistical strength theory[J]. Coal Science and Technology,2023,51(Supp.1):1–12.(in Chinese))
[20] 刘 慧,杨更社,申艳军,等. 冻融–受荷协同作用下砂岩细观损伤演化CT可视化定量表征[J]. 岩石力学与工程学报,2023,42(5):1 136–1 149.(LIU Hui,YANG Gengshe,SHEN Yanjun, et al. CT visual quantitative characterization of meso-damage evolution of sandstone under freeze-thaw-loading synergistic effect[J]. Chinese Journal of Rock Mechanics and Engineering,2023,42(5):1 136–1 149. (in Chinese))
[21] 王相龙,潘结南,王 凯,等. 微米CT扫描尺度下构造煤微裂隙结构特征及其对渗透性的控制[J]. 煤炭学报,2023,48(3):1 325–1 334. (WANG Xianglong,PAN Jienan,WANG Kai,et al. Characteristics of micro-CT scale pore-fracture of tectonic ally deformed coal and their controlling effect on permeability[J]. Journal of China Coal Society,2023,48(3):1 325–1 334.(in Chinese))
[22] 石建行,冯增朝,周 动,等. 基于不同热解方式下烟煤裂隙结构演化的对比[J]. 煤炭学报,2023,48(9):3 460–3 470.(SHI Jianxing,FENG Zengchao,ZHOU Dong,et al. Comparative study on the evolution of fracture structure of bituminous coal based on different pyrolysis methods[J]. Journal of China Coal Society,2023,48(9):3 460–3 470.(in Chinese))
[23] ZHOU X Y,XIA K,LI X B,et al. Suggested methods for determining the dynamic strength parameters and mode-I fracture toughness of rock materials[J]. International Journal of Rock Mechanics and Mining Sciences,2011,49(1):105–112.
[24] 王 磊,袁秋鹏,谢广祥,等. 冲击载荷下煤样能量耗散与破碎分形的长径比效应[J]. 煤炭学报,2022,47(4):1 534–1 546.(WANG Lei,YUAN Qiupeng,XIE Guangxiang,et al. Length-diameter ratio effect of energy dissipation and fractals of coal samples under impact loading[J]. Journal of China Coal Society,2022,47(4):1 534–1 546. (in Chinese))
[25] 王 磊,张 帅,刘怀谦,等. 冲击载荷下含瓦斯煤力学特性与破坏特征[J]. 采矿与安全工程学报,2023,40(6):1 323–1 334. (WANG Lei,ZHANG Shuai,LIU Huaiqian,et al. Mechanical properties and damage characteristics of gas-bearing coal under impact loading[J]. Journal of Mining and Safety Engineering,2023,40(6):1 323–1 334.(in Chinese))
[26] 王 磊,王安铖,陈礼鹏,等. 含瓦斯煤循环冲击动力学特性与裂隙扩展特征[J]. 岩石力学与工程学报,2023,42(11):2 628–2 642. (WANG Lei,WANG Ancheng,CHEN Lipeng,et al. Dynamic characteristics and crack propagation characteristics of gas-bearing coal under cyclic impact[J]. Chinese Journal of Rock Mechanics and Engineering,2023,42(11):2 628–2 642.(in Chinese))
[27] 王守光,穆鹏宇,王嘉敏,等. CT扫描的煤岩面裂隙椭球模型重构与张量表征及其应用[J]. 煤炭学报,2022,47(7):2 593–2 608. (WANG Shouguang,MU Pengyu,WANG Jiamin,et al. Ellipsoid reconstruction and tensor characterization of planar fractures in coal obtained by CT-scanning and the applications[J]. Journal of China Coal Society,2022,47(7):2 593–2 608.(in Chinese))
[28] 翟盛锐. 考虑孔隙瓦斯劣化作用的煤岩损伤本构模型[J]. 中国安全生产科学技术,2014,10(2):16–21.(ZHAI Shengrui. Constitutive model of coal or rock damage related to pore gas degradation[J]. Journal of Safety Science and Technology,2014,10(2):16–21.(in Chinese))
[29] 王登科,张 航,魏建平,等. 基于工业CT扫描的瓦斯压力影响下含瓦斯煤裂隙动态演化特征[J]. 煤炭学报,2021,46(11):3 550–3 564.(WANG Dengke,ZHANG Hang,WEI Jianping,et al. Dynamic evolution characteristics of fractures in gas?bearing coal under the influence of gas pressure using industrial CT scanning technology[J]. Journal of China Coal Society,2021,46(11):3 550–3 564.(in Chinese))
[30] 朱昌星,孙家鑫,王彦伟,等. 基于CT扫描单轴压缩下注浆体试块裂隙动态演化过程试验研究[J]. 岩土力学,2022,43(9):2 493–2 503. (ZHU Changxing,SUN Jiaxin,WANG Yanwei. Experimental study of fracture dynamic evolution process of grouting specimen under uniaxial compression based on CT scanning[J]. Rock and Soil Mechanics,2022,43(9):2 493–2 503.(in Chinese))
[31] WANG D K,ZENGF C,WEI J P,et al. Quantitative analysis offracture dynamic evolution in coal subjected to uniaxial and triaxial compression loads based on industrial CT and fractal theory[J]. Journal of Petroleum Science and Engineering,2020,196:108051.
[32] WANG G,QIN X,SHEN J,et al. Quantitative analysis of mi-croscopic structure and gas seepage characteristics of low-rank coal based on CT three-dimensional reconstruction of CT images and fractal theory[J]. Fuel,2019,256:115900.
[33] 唐一举,郝天轩,刘 静,等. 瓦斯与应力作用下煤体红外辐射响应研究[J]. 岩石力学与工程学报,2023,42(3):594–605.(TANG Yiju,HAO Tianxuan,LIU Jing,et al. Infrared radiation response of coal under the action of gas and stress[J]. Chinese Journal of Rock Mechanics and Engineering,2023,42(3):594–605.(in Chinese))
[34] 郎颖娴,梁正召,董 卓. 玄武岩三维细观孔隙模型重构与直接拉伸数值试验[J]. 工程科学学报,2019,41(8):997–1 006.(LANG Yingxian,LIANG Zhengzhao,DONG Zhuo. Three-dimensional microscopic model reconstruction of basalt and numerical direct tension tests[J]. Chinese Journal of Engineering,2019,41(8):997–1 006.(in Chinese))
[35] 王 磊,陈礼鹏,刘怀谦,等. 不同初始瓦斯压力下煤体动力学特性及其劣化特征[J]. 岩土力学,2023,44(1):144–158.(WANG Lei,CHEN Lipeng,LIU Huaiqian,et al. Dynamic behaviors and deterioration characteristics of coal under different initial gas pressures[J]. Rock and Soil Mechanics,2023,43(9):144–158.(in Chinese))