砂岩矿物组分流变特性纳米压痕实验研究

doi:10.13722/j.cnki.jrme.2020.0477

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Abstract In deep underground engineering，the rheological characteristics of rock can affect the construction design and stabilities of engineering structures，which has been extensively investigated. However，the previous studies mainly focused on large inhomogeneous rock samples and ignored the rheological characteristics of minerals in them at the meso-scale. Consequently，in this study，the rheological characteristics and constitutive model of various minerals in sandstone were investigated by using the nanoindentation technique. The distributions of minerals were obtained by using X-ray diffraction(XRD)，scanning electron microscope(SEM) and energy dispersive spectrometer(EDS). The elastic moduli of quartz，albite，calcite and kaolinite from nanoindentation experiment are respectively 87.74，59.85，32.30 and 17.31 GPa，indicating the heterogeneity of the sandstone at the meso-scale. The nanoindentation rheological process consists of instantaneous elastic deformation，creep and elastic aftereffect，which can be described by the Burgess model. During the rheological process，the creep load-holding and unloading periods inevitably make the pores and cracks in the minerals develop，which aggravates the deformation during elastic aftereffect and yields smaller rheological parameters than those obtained from the creep. The macro-scale rheological elastic parameters of sandstone can be obtained by upgrading the rheological elastic parameters of its mineral components at the meso-scale，which provides a convenient and efficient method for studying the rheological properties of sandstone.

Key words： rock mechanics sandstone rheological characteristics constitutive model nanoindentation upscaling

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	Articles by authors
	SUN Changlun1
	2
	LI Guichen1
	2
	XU Jiahui1
	2
	RONG Haoyu1
	2
	SUN Yuantian1
	2

Cite this article:

SUN Changlun1,2,LI Guichen1, et al. Rheological characteristics of mineral components in sandstone based on nanoindentation[J]. , 2021, 40(1): 77-87.

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https://rockmech.whrsm.ac.cn/EN/10.13722/j.cnki.jrme.2020.0477 OR https://rockmech.whrsm.ac.cn/EN/Y2021/V40/I1/77

[1] 赵阳升. 矿山岩石流体力学[M]. 北京：煤炭工业出版社，1994：1–3.(ZHAO Yangsheng. Fluid mechanics of mining rocks[M]. Beijing：China Coal Industry Publishing House，1994：1–3.(in Chinese))
[2] 何满潮，谢和平，彭苏萍，等. 深部开采岩体力学研究[J]. 岩石力学与工程学报，2005，24(16)：2 803–2 813.(HE Manchao，XIE Heping，PENG Suping，et al. Study on rock mechanics in deep mining engineering[J]. Chinese Journal of Rock Mechanics and Engineering，2005，24(16)：2 803–2 813.(in Chinese))
[3] 孙钧. 岩石流变力学及其工程应用研究的若干进展[J]. 岩石力学与工程学报，2007，26(6)：6–31.(SUN Jun. Rock rheological mechanics and its advance in engineering applications[J]. Chinese Journal of Rock Mechanics and Engineering，2007，26(6)：6–31.(in Chinese))
[4] 姚强岭，朱柳，黄庆享，等. 含水率对细粒长石岩屑砂岩蠕变特征影响试验研究[J]. 采矿与安全工程学报，2019，36(5)：1 034–1 042. (YAO Qiangling，ZHU Liu，HUANG Qingxiang， et al. Experimental study on the effect of moisture content on creep characteristics of fine-grained feldspar lithic sandstone[J]. Journal of Mining and Safety Engineering，2019，36(5)：1 034–1 042.(in Chinese))
[5] SONE H，ZOBACK M D. Time-dependent deformation of shale gas reservoir rocks and its long-term effect on the in-situ state of stress[J]. International Journal of Rock Mechanics and Mining Sciences，2014，69：120–132.
[6] 赵宝云，刘东燕，朱可善，等. 重庆红砂岩单轴直接拉伸蠕变特性试验研究[J]. 岩石力学与工程学报，2011，30(增2)：3 960–3 965. (ZHAO Baoyun，LIU Dongyan，ZHU Keshan，et al. Uniaxial compressive creep test of red sandstone and its constitutive model[J]. Chinese Journal of Rock Mechanics and Engineering，2011，30(Supp.2)：3 960–3 965.( in Chinese))
[7] JIA C J，XU W Y，WANG R B，et al. Experimental investigation on shear creep properties of undisturbed rock discontinuity in Baihetan Hydropower Station[J]. International Journal of Rock Mechanics and Mining Sciences，2018；104：27–33.
[8] KALEI G N. Some results of microhardness test using the depth of impression[J]. Mashinovedenie，1968，4(3)：105–107.
[9] LI X，BHUSHAN B. A review of nanoindentation continuous stiffness measurement technique and its applications[J]. Materials Characterization，2002，48(1)：11–36.
[10] FISCHER-CRIPPS A C. A simple phenomenological approach to nanoindentation creep[J]. Materials Science and Engineering A，2004，385(1/2)：74–82.
[11] HACKNEY S A，AIFANTIS K E，TANGTRAKARN A，et al. Using the Kelvin-Voigt model for nanoindentation creep in Sn-C/PVDF nanocomposites[J]. Materials Science and Technology，2012，28(9/10)：1 161–1 166.
[12] SHEPHERD T N，ZHANG J，OVAERT T C，et al. Direct comparison of nanoindentation and macroscopic measurements of bone viscoelasticity[J]. Journal of the Mechanical behavior of Biomedical Materials，2011，4(8)：2 055–2 062.
[13] LIU K，OSTADHASSN M，BUBACH B. Applications of nano- indentation methods to estimate nanoscale mechanical properties of shale reservoir rocks[J]. Journal of Natural Gas Science and Engineering，2016，35：1 310–1 319.
[14] 时贤，蒋恕，卢双舫，等. 利用纳米压痕实验研究层理性页岩岩石力学性质——以渝东南酉阳地区下志留统龙马溪组为例[J]. 石油勘探与开发，2019，46(1)：155–164.(SHI Xian，JIANG Shu，LU Shuangfang，et al. Investigation of mechanical properties of bedded shale by nanoindentation tests：a case study on lower silurian Longmaxi formation of Youyang area in southeast Chongqing，China[J]. Petroleum Exploration and Development，2019，46(1)：155–164.(in Chinese))
[15] SUN C，LI G，GOMAH M E，et al. Meso-scale mechanical properties of mudstone investigated by nanoindentation[J]. Engineering Fracture Mechanics，2020，238：107245.
[16] 孙长伦，李桂臣，ELGHARIB G M，等. 基于纳米压痕技术的破碎煤样力学特性实验研究[J]. 煤炭学报，2020，DOI：https：//doi.org/10.13225/j.cnki.jccs.2020.0351.(SUN Changlun，LI Guichen，GOMAH M E，et al. Experimental investigation on the mechanical properties of crushed coal samples based on the nanoindentation technique[J]. Journal of China Coal Society，2020，https：//doi.org/10.13225/ j.cnki.jccs.2020.0351.(in Chinese))
[17] 张帆，郭翰群，赵建建，等. 花岗岩微观力学性质试验研究[J]. 岩石力学与工程学报，2017，36(增2)：3 864–3 872.(ZHANG Fan，GUO Hanqun，ZHAO Jianjian，et al. Experimental study of micro- mechanical properties of granite[J]. Chinese Journal of Rock Mechanics and Engineering，2017，36(Supp.2)：3 864–3 872.(in Chinese))
[18] LIU K，OSTADHASSAN M，BUBACH B. Application of nanoindentation to characterize creep behavior of oil shales[J]. Journal of Petroleum Science and Engineering， 2018，167：729–736.
[19] SLIM M，ABEDI S，BRYNDZIA L T，et al. Role of organic matter on nanoscale and microscale creep properties of source rocks[J]. Journal of Engineering Mechanics，2019，145(1)：04018121.
[20] SUN C，LI G，ZHANG S，et al. Mechanical and heterogeneous properties of coal and rock quantified and mapped at the microscale[J]. Applied Sciences，2020，10：342.
[21] SUN C，LI G，GOMAH M E et al. Creep characteristics of coal and rock investigated by nanoindentation[J]. International Journal of Mining Science and Technology，2020，DOI：https：//doi.org/10.1016/ j. ijmst. 2020，08.001.
[22] HU C，LI Z. A review on the mechanical properties of cement-based materials measured by nanoindentation[J]. Construction and Build Materials，2015，90：80–90.
[23] OLIVER WC，PHARR GM. An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments[J]. Journal of Materials Research，1992，7(6)：1 564–1 583.
[24] MAYO M J，NIX W D. A micro-indentation study of superplasticity in Pb，Sn，and Sn-38 wt% Pb[J]. Acta Metallurgica. 1988，36(8)：2 183–2 192.
[25] 蔡美峰. 岩石力学与工程 [M]. 2版. 北京：科学出版社，2013：180–199.(CAI Meifeng. Rock mechanics and engineering[M]. 2nd，ed. Beijing：Science Press，2013：180–199.(in Chinese))
[26] 陈平，韩强，马天寿，等. 基于微米压痕实验研究页岩力学特性[J]. 石油勘探与开发，2015，42(5)：662–670.(CHEN Ping，HAN Qiang，MA Tianshou，et al. The mechanical properties of shale based on micro-indentation test[J]. Petroleum Exploration and Development 2015；42(5)：662–670.(in Chinese))