(1. State Key Laboratory of Mining Response and Disaster Prevention and Control in Deep Coal Mine,Anhui University of Science and Technology,Huainan,Anhui 232001,China;2. Engineering Research Center of Mine Underground Projects,Ministry of Education,Anhui University of Science and Technology,Huainan,Anhui 232001,China;3. School of Civil Engineering and Architecture,Anhui University of Science and Technology,Huainan,Anhui 232001,China)
Abstract:In order to investigate the physicochemical damage mechanism and dynamic mechanical properties of annular sandstone specimens under weak acid environment,the specimens of annular sandstone with outer diameter of 50 mm and inner diameters of 0,5,10,15,20 and 25 mm were corroded by weak acid solution(pH = 5) for 28 d,and the basic physical parameters,mineral compositions and microstructures were tested,and impact compression tests were carried out by using split Hopkinson pressure bar(SHPB) test device. The impact compression test was carried out using SHPB test device. The results show:Corrosion of the annular sandstone specimen by a weak acid solution produced Na+,Al3+,Fe3+,and precipitates such as silicic acid(H2SiO3);Specimen mass loss rate,volume expansion rate and density reduction rate all increase with increasing pore size;with increasing pore size of annular sandstone specimens,the dynamic compressive strength and dynamic elastic modulus show a decreasing trend of exponential function,the dynamic peak strain and the average strain rate show a quadratic and linear trend of increasing,respectively,and the degree of specimen impact crushing is intensified;Compared with the specimens of annular sandstone specimens eroded by neutral solution(pH = 7),the specimens showed a decrease in dynamic compressive strength and dynamic elastic modulus,and an increase in dynamic strain and average strain rate. The acid-rock reaction causes the sandstone to generate new substances,and the larger the pore size,the easier it is for acid ions to enter the interior of the specimen,and the more serious the deterioration of its structural damage is,resulting in a significant decrease in the kinetic properties.
[1] 袁 亮,王恩元,马衍坤,等. 我国煤岩动力灾害研究进展及面临的科技难题[J]. 煤炭学报,2023,48(5):1 825–1 845.(YUAN Liang,WANG Enyuan,MA Yankun,et al. Research progress of coal and rock dynamic disasters and scientific and technological problems in China[J]. Journal of China Coal Society,2023,48(5):1 825–1 845.(in Chinese))
[2] PING Q,WU S,LI X,et al. Dynamic and energy consumption characteristics of sandstone ring specimens under dry and wet cycling[J]. Applied Sciences,2024,14(6):2 646.
[3] PING Q,WU Y,GAO Q,et al. Experimental study on dynamic characteristics of annular coal mine sandstone after different temperatures[J]. Advances in Civil Engineering,2022,2022:1–10.
[4] 平 琦,高 祺,王 晨. 不同内径圆环砂岩试件温水耦合动态劈裂力学试验研究[J]. 振动与冲击,2023,42(17):43–51.(PING Qi,GAO Qi,WANG Chen. Experimental study on thero-water coupled dynamic splitting of annular sandstone specimens with different inner diameters[J]. Vibration and Shock,2023,42(17):43–51.(in Chinese))
[5] 辛宏举,范宝明,张海娜,等. 岩石圆环试样对径压缩破坏的数值模拟研究[J]. 力学与实践,2021,43(6):861–866.(XIN Hongju,FAN Baoming,ZHANG Haina,et al. Numerical simulation study of buttress compression damage of rock circular specimens[J]. Mechanics and Practice,2021,43(6):861–866.(in Chinese))
[6] 王 春,王怀彬,熊祖强,等,温湿循环条件下圆环花岗岩径向压缩力学特征试验研究[J]. 岩石力学与工程学报,2020,39(增2):3 260–3 270.(WANG Chun,WANG Huaibin,XIONG Zuqiang,et al. Experimental study on mechanical characteristics of radial compression of circular granite under the condition of temperature-humidity cycling[J]. Chinese Journal of Rock Mechanics and Engineering,2020,39(Supp.2):3 260–3 270.(in Chinese))
[7] 杨圣奇,李 尧,黄彦华,等. 单孔圆盘劈裂试验宏细观力学特性颗粒流分析[J]. 中国矿业大学学报,2019,48(5):984–992.(YANG Shengqi,LI Yao,HUANG Yanhua,et al. Particle flow analysis of macroscopic and microscopic mechanical properties of Brazilian disc containing a hole under splitting test[J]. Journal of China University of Mining and Technology,2019,48(5):984–992.(in Chinese))
[8] 骆 韬,郭保华,焦 峰,等. 水化学作用对砂岩力学性质影响试验研究[J]. 地下空间与工程学报,2019,15(5):1 316–1 322.(LUO Tao,GUO Baohua,JIAO Feng,et al. The Influence of hydrochemical erosion on the mechanical characteristics of sandstone[J]. Chinese Journal of Underground Space and Engineering,2019,15(5):1 316–1 322.(in Chinese))
[9] 邓 鹏,杨春和,郭印同,等. 川东北碳酸盐岩酸化损伤及力学特性试验研究[J]. 地下空间与工程学报,2019,15(3):708–718. (DENG Peng,YANG Chunhe,GUO Yintong,et al. Experimental study on damage mechanical characteristics of carbonate rock with acid treatments in northeast Sichuan[J]. Chinese Journal of Underground Space and Engineering,2019,15(3):708–718.(in Chinese))
[10] 苗胜军,蔡美峰,冀 东,等. 酸性化学溶液作用下花岗岩力学特性与参数损伤效应[J]. 煤炭学报,2016,41(4):829–835.(MIAO Shengjun,CAI Meifeng,JI Dong,et al. Damage effect of granite?s mechanical properties and parameters under the action of acidic solutions[J]. Journal of China Coal Society,2016,41(4):829–835.(in Chinese))
[11] 王艳磊,唐建新,江 君,等. 水–岩化学作用下灰砂岩的力学特性与参数损伤效应[J]. 煤炭学报,2017,42(1):227–235.(WANG Yanlei,TANG Jianxin,JIANG Jun,et al. Mechanical properties and parameter damage effects of malmstone under chemical corrosion of water-rock interaction[J]. Journal of China Coal Society,2017,42(1):227–235.(in Chinese))
[12] 张重远,窦子豪,周伦仕,等. 酸蚀作用对岩石裂隙剪切行为的影响规律研究[J]. 岩石力学与工程学报,2023,42(增1):3 256–3 265. (ZHANG Chongyuan,DOU Zihao,ZHOU Lunshi,et al. Effect of acid corrosion on shear behaviors of rock fractures[J]. Chinese Journal of Rock Mechanics and Engineering,2023,42(Supp.1):3 256–3 265. (in Chinese))
[13] 苗子臻,李曙光,霍润科,等. 受酸腐蚀砂岩力学特性及其统计损伤本构模型[J]. 铁道学报,2023,45(1):141–149.(MIAO Zizhen,LI Shuguang,HUO Runke,et al. Mechanical properties and statistical damage constitutive model of acid-corroded sandstone[J]. Journal of the China Railway Society,2023,45(1):141–149.(in Chinese))
[14] 陈有亮,陈奇键,肖 鹏,等. 岩石化学腐蚀–围压损伤本构模型与离散元模拟研究[J]. 固体力学学报,2022,43(6):703–715. (CHEN Youliang,CHEN Qijian,XIAO Peng,et al. Research on rock chemical corrosion-peri-compression damage intrinsic modeling and discrete element simulation[J]. Acta Mechanica Solida Sinica,2022,43(6):703–715.(in Chinese))
[15] 张淑坤,王来贵,唐楠楠. 化学腐蚀–冻融条件下加载岩石能量演化规律及耗散模型研究[J]. 中国安全生产科学技术,2022,18(6):148–154.(ZHANG Shukun,WANG Laigui,TANG Nannan. Study on the energy evolution law and dissipation model of loaded rock under chemical corrosion and freeze-thaw conditions[J]. China Safety Production Science and Technology,2022,18(6):148–154.(in Chinese))
[16] 张站群,蔚立元,李光雷,等. 化学腐蚀后灰岩动态拉伸力学特性试验研究[J]. 岩土工程学报,2020,42(6):1 151–1 158.(ZHANG Zhanqun,WEI Liyuan,LI Guanglei,et al. Experimental research on dynamic tensile mechanics of limestone after chemical corrosion[J]. Chinese Journal of Geotechnical Engineering,2020,42(6):1 151–1 158.(in Chinese))
[17] 刘厚彬,崔 帅,孟英峰,等. 酸化前后碳酸盐岩微细观组构及力学性能研究[J]. 地下空间与工程学报,2020,16(5):1 321–1 327. (LIU Houbin,CUI Shuai,MENG Yingfeng,et al. Study on the microstructure and mechanical properties of carbonate rock before and after acidification[J]. Chinese Journal of Underground Space and Engineering,2020,16(5):1 321–1 327.(in Chinese))
[18] 于 洋,王泽华,唐才萱. 单轴压缩下酸腐蚀花岗岩能量演化与分形特征[J]. 岩土力学,2023,44(7):1 971–1 982.(YU Yang,WANG Zehua,TANG Caixuan. Energy evolution and fractal characteristics of acid corroded granite under uniaxial compression[J]. Rock and Soil Mechanics,2023,44(7):1 971–1 982.(in Chinese))
[19] 党发宁,高天晴,原诗晶,等. 化学环境对灰岩力学性能影响的纳米压痕试验研究[J]. 岩石力学与工程学报,2022,41(增2):3 260–3 270.(DANG Fanning,GAO Tianqing,YUAN Shijing,et al. Nanoindentation test study on the influence of chemical environment on the mechanical properties of limestone[J]. Chinese Journal of Rock Mechanics and Engineering,2022,41(Supp.2):3 260–3 270.(in Chinese))
[20] 李光雷,蔚立元,苏海健,等. 化学腐蚀灰岩SHPB冲击动力学性能研究[J]. 岩石力学与工程学报,2018,37(9):2 075–2 083.(LI Guanglei,WEI Liyuan,SU Haijian,et al. Dynamic properties of corroded limestone based on SHPB[J]. Chinese Journal of Rock Mechanics and Engineering,2018,37(9):2 075–2 083.(in Chinese))
[21] LIU X,WANG S,LIU B,et al. Effect of microstructure on changes to the pore structure and mechanical properties of limestone under acidic groundwater corrosion[J]. International Journal of Geomechanics.,2023,23(12):04023212.
[22] CHEN Q,CHEN Y,XIAO P,et al. Mechanical properties and damage constitutive model of sandstone after acid corrosion and high temperature treatments[J]. International Journal of Mining Science and Technology,2023,33(6):747–760.
[23] YU Y,WANG J,FENG G L,et al. Damage evolution and acoustic emission characteristics of hydrochemically corroded limestone[J]. Bulletin of Engineering Geology and the Environment,2023,82(4):112.
[24] International Society for Rock Mechanics(ISRM). Suggested methods for determining tensile strength of rock materials[J]. International Journal of Rock Mechanics and Mining Science and Geomechanics Abstracts,1978,15(15):99–103.
[25] 中华人民共和国行业标准编写组. T/CSRME 001—2019岩石动力特性试验规程[S]. 北京:中国标准出版社,2020.(The Professional Standards Compilation Groups of the People?s Republic of China. T/CSRME 001—2019 Technical specification for testing method of rock dynamic properties[S]. Beijing:Standards Press of China,2020.(in Chinese))
[26] 李夕兵,古德生. 岩石冲击动力学[M]. 长沙:中南工业大学出版社,1994:2–93.(LI Xibing,GU Desheng. Rock impact dynamics[M]. Changsha:Zhongnan University of Technology Press,1994:2–93.(in Chinese))
[27] 王礼立. 应力波基础[M]. 2 版. 北京:国防工业出版社,2010:39–64.(WANG Lili. Fundamentals of stress waves[M]. 2nd ed. Beijing:National Defense Industry Press,2010:39–64.(in Chinese))
[28] 平 琦,孙施佳,高 祺,等. 饱水裂隙砂岩动态力学特性与裂纹扩展规律研究[J].岩石力学与工程学报,2024,43(增1):3 131–3 139.(PING Qi,SUN Shijia,GAO Qi,et al. Study on dynamic mechanical properties and crack extension law of water-saturated fissured sandstone[J]. Chinese Journal of Rock Mechanics and Engineering,2024,43(Supp.1):3 131–3 139.(in Chinese))
[29] 宫凤强,李夕兵,刘希灵. 三维动静组合加载下岩石力学特性试验初探[J]. 岩石力学与工程学报,2011,30(6):1 179–1 190.(GONG Fengqiang,LI Xibing,LIU Xiling. A preliminary study on the mechanical properties of rocks under three-dimensional dynamic-static loading [J]. Chinese Journal of Rock Mechanics and Engineering,2011,30(6):1 179–1 190.(in Chinese))