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| Experimental study on evolution of meso-structure of granite subjected to high temperature |
| BU Mohua1,2,GUO Pingye1,2,JIN Xin1,2,HE Manchao1,2,WANG Jiamin3 |
(1. State Key Laboratory for Tunnel Engineering,China University of Mining and Technology(Beijing),Beijing 100083,China;
2. School of Mechanics and Civil Engineering,China University of Mining and Technology(Beijing),Beijing 100083,China;
3. Deep Mining and Rock Burst Research Institute,China Coal Research Institute,Beijing 100013,China) |
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Abstract Understanding the mesostructural evolution of high-temperature damaged granite is crucial to reveal the degradation mechanism of its macro-physical and mechanical properties. In this study,granite was treated at high temperature(25 ℃,100 ℃,200 ℃,300 ℃,400 ℃,500 ℃ and 600 ℃),and then the uniaxial compression test was carried out on the thermal-treated granite. Finally,the meso-structure of granite was qualitatively and quantitatively analyzed using optical microscope,CT scanning and nuclear magnetic resonance(NMR). The results indicate that the mechanical properties of granite are strongly dependent on temperature,and the compressive strength increases at first and then decreases with the temperature. 200 ℃ is the peak temperature of thermal strengthening effect,400 ℃ is the threshold temperature for meso structural damage of granite,and 600 ℃ is the threshold temperature of brittle-ductile transition of granite. Further analysis indicates that the high temperature leads to a denser structure of granite and the porosity decreases with temperature at 25 ℃–200 ℃. The initiation and propagation of thermally-induced cracks can be observed in granite after 300 ℃. These cracks propagate from the edge to the interior of the specimen,and the number of pores increases with the temperature,and mesopore and macropores are dominant. The porosity increases exponentially with temperature. In addition,the fractal dimension of micropores decreases with temperature,which means that high temperature simplifies the structure of micropores,while mesopores and macropores show good fractal characteristics and are not affected by temperature.
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[1] BREEDE K,DZEBISASHVILI K,LIU X. et al. A systematic review of enhanced(or engineered) geothermal systems:past,present and future[J]. Geothermal Energy,2013,(1/4):1–27.
[2] ZHU Z N,YANG S Q,RANJITH P G,et al. A comprehensive review on mechanical responses of granite in enhanced geothermal systems (EGSs)[J]. Journal of Cleaner Production,2023,383:135378.
[3] WANG F,KONIETZKY H,FRüHWIRT T,et al. Laboratory testing and numerical simulation of properties and thermal-induced cracking of eibenstock granite at elevated temperatures[J]. Acta Geotechnica,2020,15:2 259–2 275.
[4] HUANG Y H,YANG S Q,BU Y S. Effect of thermal shock on the strength and fracture behavior of pre-flawed granite specimens under uniaxial compression[J]. Theoretical and Applied Fracture Mechanics,2020,106:102474.
[5] 郭平业,卜墨华,张 鹏,等. 高地温隧道灾变机制与灾害防控研究进展[J]. 岩石力学与工程学报,2023,42(7):1 561–1 581.(GUO Pingye,BU Mohua,ZHANG Peng,et al. Review on catastrophe mechanism and disaster countermeasure of high geotemperature tunnels[J]. Chinese Journal of Rock Mechanics and Engineering. 2023,42(7):1 561–1 581.(in Chinese))
[6] 郤保平,成泽鹏,何水鑫,等. 高温后花岗岩渗透性及其演变规律试验研究[J]. 岩石力学与工程学报,2021,40(增1):2 716–2 723. (XI Baoping,CHENG Zepeng,HE Shuixin,et al. Experimental study on permeability characteristics and its evolution of granite after high temperature[J]. Chinese Journal of Rock Mechanics and Engineering,2021,40(Supp.1):2 716–2 723.(in Chinese))
[7] 郭平业,卜墨华,李清波,等. 岩石有效热导率精准测量及表征模型研究进展[J]. 岩石力学与工程学报,2020,39(10):1 983–2 013. (GUO Pingye,BU Mohua,LI Qingbo,et al. Research progress of accurate measurement and characterization model of effective thermal conductivity of rock[J]. Chinese Journal of Rock Mechanics and Engineering,2020,39(10):1 983–2 013.(in Chinese))
[8] JANSEN D P,CARLSON S R,YOUNG R P,et al. Ultrasonic imaging and acoustic emission monitoring of thermally induced microcracks in Lac du Bonnet granite[J]. Journal of Geophys Research,1993,98(B12):22 231–22 243.
[9] QIN Y,TIAN H,XU N X,et al. Physical and mechanical properties of granite after high-temperature treatment[J]. Rock Mechanics and Rock Engineering,2020,53(1):305–322.
[10] 王嘉敏,王守光,李向上,等. 热冲击花岗岩力学响应及损伤特征显微CT试验研究[J]. 煤炭科学技术,2023,51(8):58–72.(WANG Jiamin,WANG Shouguang,LI Xiangshang,et al. Study on mechanical properties and damage characteristics of granite under thermal shock based on CT scanning[J]. Coal Science and Technology,2023,51(8):58–72.(in Chinese))
[11] XU L,GONG F Q,LIU Z X. Experiments on rockburst proneness of pre-heated granite at different temperatures:Insights from energy storage,dissipation and surplus[J]. Journal of Rock Mechanics and Geotechnical Engineering,2022,14(5):1 343–1 355.
[12] WANG J M,ZHANG P,BU M H. et al. Mechanical behavior of granite subjected to thermal treatment:insight from experiment and numerical simulation[J]. Bulletin of Engineering Geology and the Environment,2023,82:400.
[13] WANG J M,ZHANG P,BU M H,et al. Mechanical behavior of granite subjected to thermal treatment:insight from experiment and numerical simulation[J]. Bulletin of Engineering Geology and the Environment,2023,82(11):400.
[14] KONG B,WANG E Y,LI Z H,et al. Fracture mechanical behavior of sandstone subjected to high-temperature treatment and its acoustic emission characteristics under uniaxial compression conditions[J]. Rock Mechanics and Rock Engineering,2016,49:4 911–4 918.
[15] LI Z H,WONG L N Y,THE C I. Influence of thermal and mechanical loading on development of microcracks in granite[J]. Rock Mechanics and Rock Engineering,2020,53:2 035–2 051.
[16] ERSOY H,KOLAYLI H,KARAHAN M,et al. Effect of thermal damage on mineralogical and strength properties of basic volcanic rocks exposed to high temperatures[J]. Bulletin of Engineering Geology and the Environment,2019,78:1 515–1 525.
[17] JIN P H,HU Y Q,SHAO J X,et al. Influence of different thermal cycling treatments on the physical,mechanical and transport properties of granite[J]. Geothermics,2019,78:118–128.
[18] ZHAO Z H,XU H R,WANG J. Auxetic behavior of Beishan granite after thermal treatment:A microcracking perspective[J]. Engineering Fracture Mechanics,2020,231:107017.
[19] 方新宇,许金余,刘 石,等. 高温后花岗岩的劈裂试验及热损伤特性研究[J]. 岩石力学与工程学报,2016,35(增1):2 687–2 694. (FANG Xinyu,XU Jinyu,LIU Shi,et al. Research on splitting-tensile tests and thermal damage of granite under post-high temperature[J]. Chinese Journal of Rock Mechanics and Engineering,2016,35(Supp.1):2 687–2 694.(in Chinese))
[20] ZHANG D K,MENG T,TAHERDANGKOO R,et al. Evolution trend and weakening mechanism of mode-I fracture characteristics of granite under coupled thermo-hydro-mechanical and thermal treatments[J]. Engineering Fracture Mechanics,2022,275: 108794.
[21] YANG S Q,RANJITH P G,JING H W,et al. An experimental investigation on thermal damage and failure mechanical behavior of granite after exposure to different high temperature treatments[J]. Geothermics,2017,65:180–197.
[22] 赵亚永,魏 凯,周佳庆,等. 三类岩石热损伤力学特性的试验研究与细观力学分析[J]. 岩石力学与工程学报,2017,36(1):142– 151.(ZHAO Yayong,WEI Kai,ZHOU Jiaqing,et al. Laboratory study and micromechanical analysis of mechanical behaviors of three thermally damaged rocks[J]. Chinese Journal of Rock Mechanics and Engineering,2017,36(1):142–151.(in Chinese))
[23] CHEN Y L,WANG S R,NI J,et al. An experimental study of the mechanical properties of granite after high temperature exposure based on mineral characteristics[J]. Engineering Geology,2017,220:234–242.
[24] LIU S,XU J Y. An experimental study on the physico-mechanical properties of two post-high-temperature rocks[J]. Engineering Geology,2015,185:63–70.
[25] SHAO S S,WASANTHA P L P,RANJITH P G,et al. Effect of cooling rate on the mechanical behavior of heated Strathbogie granite with different grain sizes[J]. International Journal of Rock Mechanics and Mining Sciences,2014,70:381–387.
[26] BU M H,ZHANG P,GUO P Y,et al. Deterioration of equivalent thermal conductivity of granite subjected to heating-cooling treatment[J]. Journal of Rock Mechanics and Geotechnical Engineering,2024,https://doi.org/10.1016/j.jrmge.2023.11.014.
[27] WU X G,HUANG Z W,SONG H Y,et al. Variations of physical and mechanical properties of heated granite after rapid cooling with liquid nitrogen[J]. Rock Mechanics and Rock Engineering,2019,52: 2 123–2 139.
[28] KUMARI W G P,RANJITH P G,PERERA M S A,et al. Temperature-dependent mechanical behaviour of Australian Strathbogie granite with different cooling treatments[J]. Engineering Geology,2017,229:31–44.
[29] SHA S,RONG G,CHEN Z H,et al. Experimental evaluation of physical and mechanical properties of geothermal reservoir rock after different cooling treatments[J]. Rock Mechanics and Rock Engineering,2020,53:4 967–4 991.
[30] WU Q H,WENG L,ZHAO Y L,et al. On the tensile mechanical characteristics of fine-grained granite after heating/cooling treatments with different cooling rates[J]. Engineering Geology,2019,253:94–110.
[31] SUNNETCI M O,ERSOY H. A new perspective based on overcoming sample heterogeneity for the estimation of thermal damage inflicted on volcanic rocks using non-destructive tests[J]. Rock Mechanics and Rock Engineering,2023,56:35–56.
[32] WONG L N Y,ZHANG Y H,CUI X,et al. Thermal effect on rock strength:strengthening-weakening transition explored by grain-based model[J]. Acta Geotechnica,2023,htps://doi.org/10.1007/s11440– 023–02049–2.
[33] TANG Z C,PENG M H,XIAO S G. Basic friction angle of granite fracture after heating and rapid cooling treatments[J]. Engineering Geology,2022,302:106626.
[34] KANG F C,LI Y C,TANG C A. Grain size heterogeneity controls strengthening to weakening of granite over high-temperature treatment[J]. International Journal of Rock Mechanics and Mining Sciences,2021,145:104848.
[35] ZHANG S K,HUANG Z W,ZHANG H Y,et al. Experimental study of thermal-crack characteristics on hot dry rock impacted by liquid nitrogen jet[J]. Geothermics,2018,76:253–260.
[36] ZHU Z N,THOMAS K,RANJITH P G,et al. Changes in thermomechanical properties due to air and water cooling of hot dry granite rocks under unconfined compression[J]. Renewable Energy,2021,170(1):562–573.
[37] ABU BAKAR M Z,ALI H,MAJEED Y. Majeed Y. Effects of heat treatment and confining pressure on rock abrasivity and its ramifications for bit wear and drillability in deep geothermal reservoirs[J]. Rock Mechanics and Rock Engineering,2023,56: 8 191–8 208.
[38] KHAN N M,Ma L Q,CAO K W,et al. Evaluating the thermal-cooling induced effects on the Ambela granite properties (from Pakistan) using experimental and image processing techniques[J]. Bulletin of Engineering Geology and the Environment,2022,81:506.
[39] WANG J T,ZUO J P,SUN Y J,et al. The effects of thermal treatments on the fatigue crack growth of Beishan granite:an in situ observation study[J]. Bulletin of Engineering Geology and the Environment,2021,80:1 541–1 555.
[40] GUO P Y,BU M H,ZHANG P,et al. Mechanical properties and crack propagation behavior of granite after high temperature treatment based on a thermo-mechanical grain-based model[J]. Rock Mechanics and Rock Engineering,2023b,56:6 411–6 435.
[41] FAN L F,GAO J W,DU X L,et al. Spatial gradient distributions of thermal shock-induced damage to granite[J]. Journal of Rock Mechanics and Geotechnical Engineering,2020,12:917–926.
[42] 赵阳升,孟巧荣,康天合,等. 显微CT试验技术与花岗岩热破裂特征的细观研究[J]. 岩石力学与工程学报,2008,27(1):28–34. (ZHAO Yangsheng,MENG Qiaorong,KANG Tianhe,et al. Micro- CT experimental technology and meso-investigation on thermal fracturing characteristics of granite[J]. Chinese Journal of Rock Mechanics and Engineering,2008,27(1):28–34.(in Chinese))
[43] ISAKA B L A,RANJITH P G,RATHNAWEERA T D,PERERA M S A,et al. Quantification of thermally-induced microcracks in granite using X-ray CT imaging and analysis[J]. Geothermics,2019,81:152–167.
[44] XI Y,XING J Y,JIANG H L,et al. Pore characteristic evolution and damage deterioration of granite subjected to the thermal and cooling treatments combined with the NMR method[J]. Bulletin of Engineering Geology and the Environment,2023,82:182.
[45] WU R Y,CHEN S W,YANG F B,et al. Experimental study on the thermal healing effect on stress-damaged Granite[J]. Rock Mechanics and Rock Engineering,2023,56:6 615–6 629.
[46] LI Q,LI X B,YIN T B. Factors affecting pore structure of granite under cyclic heating and cooling:A nuclear magnetic resonance investigation[J]. Geothermics,2021,96:102198.
[47] 任伟光. 深部煤体孔裂隙结构的多尺度分形表征及渗透机制研究[博士学位论文][D]. 北京:中国矿业大学(北京),2022.(REN Weiguang. The study on multiscale fractal characterization and permeability mechanism of pore structure in deep coal[Ph. D. Thesis][D]. Beijing:China University of Mining and Technology (Beijing),2022.(in Chinese))
[48] LIN M,WANG D M,SHAO Z L. Experimental study on changes of pore structure and mechanical properties of sandstone after high-temperature treatment using nuclear magnetic resonance[J]. Engineering Geology,2020,275:105739.
[49] CAI Y D,LIU D M,PAN Z J,et al. Petrophysical characterization of Chinese coal cores with heat treatment by nuclear magnetic resonance[J]. Fuel,2013,108:292–302.
[50] MENG F D,ZHAI Y,LI Y B,et al. Research on the effect of pore characteristics on the compressive properties of sandstone after freezing and thawing[J]. Engineering Geology,2021,286: 106088.
[51] MANDELBROT B. On the geometry of homogeneous turbulence,with stress on the fractal dimension of the iso-surfaces of scalars[J]. Journal of Fluid Mechanics,1975,72:401–416.
[52] BI J,DU C,ZHAO Y,et al. Characterization of shear behavior and damage mechanism of periodic thermal loading sandstone based on NMR technique[J]. Engineering Geology,2023,325:107272.
[53] WONG L N Y,ZHANG Y H,WU Z J. Rock strengthening or weakening upon heating in the mild temperature range?[J]. Engineering Geology,2020,272:105619.
[54] ZHANG W Q,SUN Q,HAO S Q,et al. Experimental study on the variation of physical and mechanical properties of rock after high temperature treatment[J]. Applied Thermal Engineering,2016,98: 1 297–1 304.
[55] PAVESE A,CURETTI N,DIELL V,et al. P-V and T-V Equations of State of natural biotite:an in-situ high-pressure and high temperature powder diffraction study,combined with Mössbauer spectroscopy[J]. American Mineralogist,2007,92(7):1 158–1 164.
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