摘要为综合研究花岗岩细观特征和层裂断口微观特征,利用霍普金森杆装置对花岗岩杆件进行不同冲击荷载的层裂试验,通过晶体矿物学研究矿物细观结构,利用高速摄影仪研究细观裂纹扩展,采用能谱仪(energy dispersive spectrometer,EDS)和扫描电镜(scanning electron microscopy,SEM)研究试样层裂断口面微观结构,最后运用分形原理,定量计算层裂断口的粗糙度。试验结果表明:花岗岩的矿物细观结构对层裂破坏具有重要影响,其中,长石、石英、云母作为花岗岩的主要成分,表现尤为突出;同时,这些矿物的分布也影响着细观裂纹的扩展。EDS和SEM图片的微观分析表明不同矿物具有不同的微观断裂特征,断口整体上的破碎程度和粗糙度,都有随着冲击荷载增大而增大的趋势,这种趋势在分形维数值的结果分析中得到了验证。
Abstract:To comprehensively research the characteristics of mesoscopic minerals and microscopic fractures of granite,the split Hopkinson bar(SHPB) device was employed to perform the spalling experiments of granite rods under different impact loads. The mesostructure of minerals was studied by crystal mineralogy,the meso-crack propagation was recorded by a high-speed camera,and the microstructure of the fracture surface of the samples was observed by energy dispersive spectrometer(EDS) and scanning electron microscopy(SEM). The roughness of the fracture was calculated quantitatively with the fractal principle. The experimental results show that the mesostructure of granite minerals has an important influence on the spallation failure,especially for feldspar,quartz and mica which are the main components of granite. The distribution of these minerals also affects the expansion of mesoscopic cracks. It is also demonstrated from the microscopic analysis of EDS and SEM images that different minerals present different micro-fracture characteristics and that the fragmentation degree and roughness of the fracture increase with increasing the impact load,which was greatly validated by the fractal dimension values.
[1] ANTOUN T,CURRAN D R,RAZORENOV S V,et al. Spall fracture[M]. Germany:Springer-Verlag,2003:37–49.
[2] 陶 明. 高应力岩体的动态加卸荷扰动特征与动力学机制研究[博士学位论文][D]. 长沙:中南大学,2013.(TAO Ming. Dynamic and unloading disturbance characteristics and dynamic mechanism of high-stress rock mass[Ph. D. Thesis][D]. Changsha:Central South University,2013.(in Chinese))
[3] XI T,FAN W,CHU G B,et al. Spall behavior of copper under ultra- high strain rate loading[J]. Acta Physica Sinica,2017,66(4):1–8.
[4] YANG Y,PENG Z Q,CHEN X Z,et al. Spall behaviors of high purity copper under sweeping detonation[J]. Materials Science and Engineering,2016,651(2016):636–645.
[5] 王礼立. 应力波基础[M]. 2版.北京:国防工业出版,2005:40–48.(WANG Lili. Stress wave basis[M]. 2nd ed. Beijing:National Defense Industry Publishing,2005:40–48.(in Chinese))
[6] 李夕兵,陶 明,宫凤强,等. 冲击载荷作用下硬岩层裂破坏的理论和试验研究[J]. 岩石力学与工程学报,2011,30(6):1 081–1 088. (LI Xibing,TAO Ming,GONG Fengqiang,et al. Theoretical and experimental study on crack failure of hard rock under impact loading[J]. Chinese Journal of Rock Mechanics and Engineering,2011,30(6):1 081–1 088.(in Chinese))
[7] 张 帆,郭翰群,赵建建,等. 花岗岩微观力学性质试验研究[J]. 岩石力学与工程学报,2017,36(2):3 864–3 872.(ZHANG Fan,GUO Hanqun,ZHAO Jianjian,et al. Experimental study of micro- mechanical properties of granite[J]. Chinese Journal of Rock Mechanics and Engineering,2017,36(2):3 864–3 872.(in Chinese))
[8] ZHANG G,CHEN M,LIU X,et al. Relationship between rock compositions and mechanical properties of reservoir for low-permeability reservoirs[J]. Liquid Fuels Technology,2013,31(14):1 415–1 422.
[9] ZHAO M,NING J G,ZHANG H B,et al. Study on microscopic structure and mineral composition of shallow rock using SEM[J]. Applied Mechanics and Materials,2013,303–306:2 552–2 558.
[10] ZHANG Z Z. Fractal dimension of fracture surface in rock material after high temperature[J]. Advances in Materials Science and Engineering,2015,(1):1–6.
[11] XU X L,ZHANG Z Z. Fractal characteristics of rock fracture surface under triaxial compression after high temperature[J]. Advances in Materials Science and Engineering,2016,(1):1 155–1 165.
[12] GHAMGOSAR M,ERARSLAN N. Experimental and numerical studies on development of fracture process zone(FPZ) in rocks under cyclic and static loadings[J]. Rock Mechanics and Rock Engineering,2016,49(3):893–908.
[13] ERARSLAN N,WILLIAMSD J. The damage mechanism of rock fatigue and its relationship to the fracture toughness of rocks[J]. International Journal of Rock Mechanics and Mining Sciences,2012,56:15–26.
[14] TIAN M S,LI X L. Analysis of microscopic mechanism mica schist fracture under uniaxial compression[J]. Pearl River,2015,36(6):44–46.
[15] ERARSLAN N. A Study on the evaluation of the fracture process zone in CCNBD rock samples[J]. Experimental Mechanics,2013,53(8):1 475–1 489.
[16] CHEN Y,NISHIYAMA T,ITO T. Application of image analysis to observe microstructure in sandstone and granite[J]. Resource Geology,2010,51(3):249–258.
[17] HE Z G,LI G S,TIAN S C,et al. SEM analysis on rock failure mechanism by supercritical CO2 jet impingement[J]. Journal of Petroleum Science and Engineering,2016,146:111–120.
[18] TIAN S C,SHEN M,LIU Q L,et al. SEM analysis on rock breaking mechanism by swirling-round SC-CO2 jet[J]. WJTA-IMCA Conference and Expo,2017,47(11):1–10.
[19] MINDESS S,DIAMOND S. SEM investigations of fracture surfaces using stereo pairs:II. fracture surfaces of rock-cement paste composite specimens[J]. Cement and Concrete Research,1992,22(4):678–688.
[20] YAO S F,ZHANG Z N,GE X R,et al. Correlation between fracture energy and geometrical characteristic of mesostructure of marble[J]. Rock and Soil Mechanics,2016,37(8):2 341–2 346.
[21] WRIGHT J S. The spalling of overgrowths during experimental freeze–thaw of a quartz sandstone as a mechanism of quartz silt production[J]. Micron,2000,31(6):631–638.
[22] PARK J,HYUN C U,PARK H D. Changes in microstructure and physical properties of rocks caused by artificial freeze-thaw action[J]. Bulletin of Engineering Geology and the Environment,2015,74(2):555–565.
[23] FEREIDOONI D. Determination of the geotechnical characteristics of horn felsic rocks with a particular emphasis on the correlation between physical and mechanical properties[J]. Rock Mechanics and Rock Engineering,2016,49(7):2 595–2 608.
[24] ZHANG G Q,CHEN M,LIU X X,et al. Relationship between rock compositions and mechanical properties of reservoir for low-permeability reservoirs[J]. Liquid Fuels Technology,2013,31(14):1 414–1 422.
[25] 李夕兵. 岩石动力学基础与应用[M]. 北京:科学出版社,2014:91–99.(LI Xibing. Foundation and application of rock dynamics[M]. Beijing:Science Press,2014:91–99.(in Chinese))
[26] 赫 尔. 断口形貌学观察、测量和分析断口表面形貌的科学[M]. 北京:科学出版社,2009:19–22.(HUL L. Fracture morphology observation,measurement and analysis of the surface morphology of fractures[M]. Beijing:Science Press,2009:19–22.(in Chinese))
[27] KINSNER W,DHAVACHELVAN P. A unified approach to fractal dimensions[J]. Journal of Information Technology Research,2005:58–72.