(1. School of Civil Engineering,Shaoxing University,Shaoxing,Zhejiang 312000,China;2. Key Laboratory of Rock Mechanics and Geohazards of Zhejiang Province,Shaoxing University,Shaoxing,Zhejiang 312000,China;3. State Key Laboratory for Tunnel Engineering,China University of Mining and Technology(Beijing),Beijing 100083,China)
Abstract:Mineral composition is an important factor affecting the macro-micro friction mechanical properties of rock. The macro-micro friction properties of sandstone are studied based on direct shear and nano-scratch tests,the variations of mineral compositions before and after shearing are analyzed using X-ray diffraction,the macro-micro friction coefficients of the rock,different minerals and their interfaces are statistically obtained,and the friction correlation mechanism between these factors is established. The results show that the proportion of hard-phase minerals in the total amount of powder increases after shearing,the proportion of soft-phase minerals decreases. The scratch depth and friction force of hard-phase minerals remain stable,those of soft-phase minerals vary significantly. Statistical analysis of the frequency distribution curve of the friction coefficient reveals that each mineral and interface exhibit a single-peak Gaussian distribution. Combined with the analysis of macro-micro friction mechanisms,it is found that the macro friction force of sandstone is influenced by surface asperities and the wear between different minerals,the friction force of hard-phase minerals primarily depends on their inherent properties,the friction force of soft-phase minerals and interfaces is affected by their inherent properties,plastic flow and the extrusion of surrounding minerals. By further quantifying the relationship between macro-micro friction coefficients,the hard-soft phase interface is found to contribute the most to the macro friction coefficient,accounting for 52.1%. The research results of the macro-micro friction properties can provide a theoretical foundation for revealing the mechanism of cross-scale friction mechanics.
[1] CHEN X F. Rock friction and dynamic faulting at the micro-to nano-scales[Ph. D. Theses][D]. Oklahoma:University of Oklahoma,2015.
[2] YANG L,ZHANG M,JIAO W Z,et al. Influence of intergranular friction weakening on rock avalanche dynamics[J]. Computers and Geotechnics,2023,159:1–16.
[3] DU K,LUO X Y,ZHOU T. Influence of textural characteristics and mineral composition on the acoustic behavior under acoustic integrated uniaxial compression[J]. Bulletin of Engineering Geology and the Environment,2023,82(9):1–16.
[4] YAO Q L,YU L Q,LI X H,et al. The effects of micro-and meso-scale characteristics on the mechanical properties of coal-bearing sandstone[J]. Arabian Journal of Geosciences,2020,13:1–18.
[5] LIU K Q,JIN Z J,ZAKHAROVA N,et al. Comparison of shale fracture toughness obtained from scratch test and nanoindentation test[J]. International Journal of Rock Mechanics and Mining Sciences,2023,162:1–12.
[6] XIN P,WANG L Q,LIU Z,et al. Structural properties of shear zone materials of the Neogene soft-rock landslides in the northeastern margin of the Tibetan Plateau[J]. Bulletin of Engineering Geology and the Environment,2021,80(6):4 277–4 290.
[7] 雍 睿,胡新丽,唐辉明,等. 岩体结构面直剪试验制样误差效应研究[J]. 中南大学学报:自然科学版,2013,44(11):4 643–4 651. (YONG Rui,HU Xinli,TANG Huiming,et al. Effect of sample preparation error on direct shear test of rock mass discontinuities[J]. Journal of Central South University:Science and Technology,2013,44(11):4 643–4 651.(in Chinese))
[8] 黄 曼,杜时贵,罗战友,等. 基于多尺度直剪试验的岩石模型结构面抗剪强度特征研究[J]. 岩土力学,2013,34(11):3 180–3 186. (HUANG Man,DU Shigui,LUO Zhanyou,et al. Study of shear strength characteristics of simulation rock structural planes based on multi-size direct shear tests[J]. Rock and Soil Mechanics,2013,34(11):3 180–3 186.(in Chinese))
[9] YAN W,WU T,WU J S,et al. Sliding frictional characteristic of tight sandstone and its influence on the hydraulic fracture complexity[J]. Geomechanics and Geophysics for Geo-Energy and Geo-Resources,2023,9(1):1–19.
[10] KOHLI A H,ZOBACK M D. Frictional properties of shale reservoir rocks[J]. Journal of Geophysical Research Solid Earth,2013,118(9):5 109–5 125.
[11] FAGERENG A,IKARI M J. Low-temperature frictional characteristics of Chlorite-Epidote-Amphibole assemblages:Implications for strength and seismic style of retrograde fault zones[J]. Journal of Geophysical Research:Solid Earth,2020,125(4):1–16.
[12] ZHANG C Q,ZHANG L S,TAO Z G,et al. Study on rock type effect of fault sliding stability[J]. Rock Mechanics and Rock Engineering,2024,57(3):1 915–1 938.
[13] RAMANA Y V,GOGTE B S. Dependence of coefficient of sliding friction in rocks on lithology and mineral characteristics[J]. Engineering Geology,1989,26(3):271–279.
[14] COX S,IKARI M J,MACLEOD C J,et al. Frictional characteristics of oceanic transform faults:Progressive deformation and alteration controls seismic style[J]. Geophysical Research Letters,2021,48(24):1–11.
[15] LIU B,XU Z W,CHEN C,et al. Numerical and experimental investigation on ductile deformation and subsurface defects of monocrystalline silicon during nano-scratching[J]. Applied Surface Science,2020,528:1–8.
[16] ZHU J X,AGHABABAEI R. On the size effect in scratch and wear response of single crystalline copper[J]. Tribology International,2023,186:1–8.
[17] LIU J,JIANG H,CHENG Q,et al. Investigation of nano-scale scratch and stick-slip behaviors of polycarbonate using atomic force microscopy[J]. Tribology International,2018,125:59–65.
[18] HU J H,HE Y,LI Z,et al. On the deformation mechanism of SiC under nano-scratching:An experimental investigation[J]. Wear,2023,522:1–10.
[19] ZHAO S K,XU X W,YANG L,et al. Investigation on the mechanical properties of shale subjected to different conditions based on nanoindentation experiments and numerical simulation[J]. Case Studies in Construction Materials,2022,17:1–18.
[20] LI Q Y,TULLIS T E,GOLDSBY D,et al. Frictional ageing from interfacial bonding and the origins of rate and state friction[J]. Nature,2011,480(7376):233–236.
[21] 郑 爽,雍 睿,杜时贵,等. 基于纳米划痕试验的砂岩结构面宏–微观摩擦因数关系研究[J]. 岩土力学,2023,44(4):1 022–1 034. (ZHENG Shuang,YONG Rui,DU Shigui,et al. Relationship between macro and micro friction coefficients of sandstone structural surface based on nano-scratch test[J]. Rock and Soil Mechanics,2023,44(4):1 022–1 034.(in Chinese))
[22] 黄 曼,刘海俊,洪陈杰,等. 考虑压痕尺寸效应的岩石矿物摩擦特性研究[J]. 岩石力学与工程学报,2024,43(6):1 371–1 382. (HUANG Man,LIU Haijun,HONG Chenjie,et al. Study on friction characteristics of rock minerals considering indentation size effect[J]. Chinese Journal of Rock Mechanics and Engineering,2024,43(6):1 371–1 382.(in Chinese))
[23] ZENG Y J,GUO Y T,ZHANG X,et al. Study on the influence of mechanical characteristics of multi-rhythm inter-salt shale oil on fracture propagation in Qianjiang formation,China[J]. Journal of Petroleum Exploration and Production Technology,2023,13(2):735–751.
[24] YANG L,YANG D,ZHANG M Y,et al. Application of nano-scratch technology to identify continental shale mineral composition and distribution length of bedding interfacial transition zone—A case study of Cretaceous Qingshankou formation in Gulong Depression,Songliao Basin,NE China[J]. Geoenergy Science and Engineering,2024,234:1–16.
[25] ULUSAY R. The ISRM suggested methods for rock characterization,testing and monitoring:2007–2014[M]. New York:Spring,2015:131–141.
[26] 雍 睿,钟 祯,杜时贵,等. 岩体结构面基本摩擦角研究现状与展望[J]. 岩石力学与工程学报,2022,41(2):254–270.(YONG Rui,ZHONG Zhen,DU Shigui,et al. Review on research advance of basic friction angle of rock joints[J]. Chinese Journal of Rock Mechanics and Engineering,2022,41(2):254–270.(in Chinese))
[27] LIU K Q,OSTADHASSAN M,BUBACH B. Applications of nano-indentation methods to estimate nanoscale mechanical properties of shale reservoir rocks[J]. Journal of Natural Gas Science and Engineering,2016,35:1 310–1 319.
[28] 孙长伦,李桂臣,许嘉徽,等. 砂岩矿物组分流变特性纳米压痕实验研究[J]. 岩石力学与工程学报,2021,40(1):77–87.(SUN Changlun,LI Guichen,XU Jiahui,et al. Rheological characteristics of mineral components in sandstone based on nanoindentation[J]. Chinese Journal of Rock Mechanics and Engineering,2021,40(1):77–87.(in Chinese))
[29] MILLER M,BOBKO C,VANDAMME M,et al. Surface roughness criteria for cement paste nanoindentation[J]. Cement and Concrete Research,2008,38(4):467–476.
[30] 钟月曦,周皓月,姚雪萍,等. 无氧铜微纳米划痕测试过程影响因素仿真研究[J]. 工程与试验,2020,60(3):35–38.(ZHONG Yuexi,ZHOU Haoyue,YAO Xueping,et al. Simulation study on the effect factors of Oxygen-Free Copper during nano-micro scratching tests[J]. Engineering and Test,2020,60(3):35–38.(in Chinese))
[31] YANG M Q,HE Z Q,LI C,et al. Experimental study on physical characteristics of deep rocks at different depths in Songliao Basin[J]. Geofluids,2022,2022(1):1–12.
[32] LU Y Q,LI C,HE Z Q,et al. Variations in the physical and mechanical properties of rocks from different depths in the Songliao Basin under uniaxial compression conditions[J]. Geomechanics and Geophysics for Geo-Energy and Geo-Resources,2020,6:1–14.
[33] DURST K,GÖKEN M,VEHOFF H. Finite element study for nanoindentation measurements on two-phase materials[J]. Journal of materials Research,2004,19(1):85–93.
[34] WEI Y,KONG W K,WANG Y Q,et al. Multifunctional application of nanoscratch technique to characterize cementitious materials[J]. Cement and Concrete Research,2021,140:1–13.
[35] LIU J H,ZENG Q,XU S L. The state-of-art in characterizing the micro/nano-structure and mechanical properties of cement-based materials via scratch test[J]. Construction and Building Materials,2020,254:1–18.
[36] BRACE F P,TABOR D. The friction and lubrication of solids[M]. Oxford:Clarendon Press,1964:60–62.
[37] 韩文梅. 岩石摩擦滑动特性及其影响因素分析[博士学位论文][D]. 太原:太原理工大学,2012.(HAN Wenmei. The study of frictional sliding characters of rocks and its influencing factors[Ph. D. Theses][D]. Taiyuan:Taiyuan University of Technology,2012.(in Chinese))